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Hooked on PChem Lab: Physical Chemistry Laboratory Manual New edition [Pehme köide]

  • Formaat: Paperback / softback, 258 pages, kõrgus x laius x paksus: 279x216x13 mm
  • Ilmumisaeg: 04-Jan-2010
  • Kirjastus: Kendall/Hunt Publishing Co ,U.S.
  • ISBN-10: 0757574475
  • ISBN-13: 9780757574474
Hooked on PChem Lab: Physical Chemistry Laboratory Manual New editionSuurem pilt
  • Formaat: Paperback / softback, 258 pages, kõrgus x laius x paksus: 279x216x13 mm
  • Ilmumisaeg: 04-Jan-2010
  • Kirjastus: Kendall/Hunt Publishing Co ,U.S.
  • ISBN-10: 0757574475
  • ISBN-13: 9780757574474
Püsilink: https://www.kriso.ee/db/9780757574474.html
Acknowledgments xvii
Chapter the First Expectations and Policies
1(20)
1.1 General
1(5)
1.1.1 Opening Thoughts
1(1)
1.1.2 Books and Reference Materials
2(1)
1.1.3 Teaching Assistants
3(1)
1.1.4 The First Day of Lab
3(1)
1.1.5 The Experiments and Scheduling
4(1)
1.1.6 Computers
5(1)
1.2 Academic Integrity
6(1)
1.3 Grading Policy
7(1)
1.4 Laboratory Procedures
8(1)
1.4.1 Pre-lab Preparation
8(1)
1.4.2 Equipment
8(1)
1.4.3 Shut Down
8(1)
1.4.4 Turn-in Procedures and Late Policies
9(1)
1.5 Lab Reports
9(8)
1.5.1 General Format Guidelines
9(2)
1.5.2 Basic Reports
11(2)
1.5.3 Formal Report Format
13(3)
1.5.4 Error Analysis
16(1)
1.6 Basic Safety and Waste Disposal Procedures
17(4)
1.6.1 Personal Safety
17(2)
1.6.2 Lab Safety
19(1)
1.6.3 Waste Disposal
19(2)
Chapter the Second Policy Differences for the Second-Semester Course
21(6)
2.1 Grading
22(3)
2.1.1 Reports
22(1)
2.1.2 Prelab Quizzes
23(1)
2.1.3 Error Analyses
23(1)
2.1.4 Oral Presentation
23(1)
2.1.5 Special Project
24(1)
2.1.6 Advanced Experiments
24(1)
2.1.7 Nanolab Mini-Report
25(1)
2.1.8 Laboratory Performance
25(1)
2.2 Experiment Types
25(2)
2.2.1 Basic Experiments
25(1)
2.2.2 The Nanolab
25(1)
2.2.3 Advanced Experiments
26(1)
2.2.4 A Special Project
26(1)
Chapter the Third Common Techniques of Statistical Analysis in Science---Data, Statistics, and Graphing, Oh My!
27(38)
3.1 General
28(1)
3.1.1 Opening Thoughts
28(1)
3.1.2 It's Not That Bad, Really
28(1)
3.1.3 The Almighty' Literature Value?
29(1)
3.2 Data---The `Meat' for the Peeled Potatoes
29(12)
3.2.1 Measurement---Precision and Accuracy
31(4)
3.2.2 Basic Data Analysis
35(3)
3.2.3 Rejection of Bad Data
38(1)
3.2.4 Validation and Calibration
39(2)
3.2.5 Standard Deviation of the Mean
41(1)
3.3 Error---Not Really Wrong...
41(10)
3.3.1 Types of Error
42(2)
3.3.2 Absolute and Relative Error
44(1)
3.3.3 Error Propagation
45(6)
3.4 Graphing---A Picture Is Worth 1000 Words, IF It Is Clear
51(4)
3.4.1 Graph Format
51(1)
3.4.2 Least Squares Analysis
52(3)
3.4.3 Error Bars
55(1)
3.5 Presenting Results---Sharing Numbers Meaningfully
55(10)
3.5.1 Significant Figures
56(1)
3.5.2 Rounding Numbers
57(1)
3.5.3 Reporting Error
58(1)
3.5.4 Unit Analysis
59(6)
Chapter the Fourth Instruments and How to Use Them
65(18)
4.1 Abbe Refractometer (LV, DM2)
65(6)
4.1.1 Analog Abbe
67(1)
4.1.2 Digital Abbe
68(2)
4.1.3 Abbe Road
70(1)
4.1.4 Abbe Normal
70(1)
4.1.5 Westminster Abbey
70(1)
4.1.6 Abba
71(1)
4.2 Analytical Balance (BC, BR DM2, PG, SL)
71(1)
4.3 Autopipettes (OR)
72(1)
4.4 Cathetometer (MS2, ST)
72(2)
4.5 Computer (LabView) (BC, MF2, MK2A, OR, PB2, RV2, TD2)
74(1)
4.6 Gas Regulator (BC, GD, HC, LE2, PA, PG, RV2)
74(1)
4.7 Manometer (Mercury and Digital) (RV2, VP)
75(1)
4.8 Mel-Temp (SL)
76(1)
4.9 Oscilloscope (HC)
77(1)
4.10 Pellet Press (BC, BP)
77(1)
4.11 Thermocouple/Thermistor (BC, BP, LE2, LV, TD2)
78(1)
4.11.1 Thermocouple
78(1)
4.11.2 Thermistor
78(1)
4.12 Viscometer (PG, TV)
79(1)
4.13 Volumetric Flask (CS2, DM2, LV, ST)
79(1)
4.14 Volumetric Pipette (BC, BP, CS2, DM2, LV, OR, PG, ST)
80(3)
Chapter the Fifth GD: Gas Diffusion
83(10)
5.1 Introduction
83(1)
5.2 Textbook References
83(1)
5.3 Chemicals
84(1)
5.4 Equipment
84(2)
5.5 Safety
86(1)
5.6 Procedure
86(3)
5.6.1 Setup
86(1)
5.6.2 Filling the Mixing Chamber
87(1)
5.6.3 Gas Diffusion Measurements
88(1)
5.7 Waste Disposal
89(1)
5.8 Shut Down
89(1)
5.9 Literature Values
90(1)
5.10 Data Analysis
90(1)
5.11 Discussion Questions
91(1)
5.12 Conclusions
92(1)
Chapter the Sixth HC: The Heat Capacity Ratios of Gases
93(10)
6.1 Introduction
93(3)
6.1.1 Heat Capacity
93(1)
6.1.2 Energy Transmission and Absorption
93(1)
6.1.3 Degrees of Freedom and the Equipartition Principle
94(2)
6.2 Textbook References
96(1)
6.3 Chemicals
96(1)
6.4 Equipment
97(1)
6.5 Safety
97(1)
6.6 Procedure
98(1)
6.6.1 Setup
98(1)
6.6.2 Wavelength Measurement
98(1)
6.6.3 Frequency Measurement
99(1)
6.7 Waste Disposal
99(1)
6.8 Shut Down
99(1)
6.9 Data Analysis
99(2)
6.9.1 Calculate the Speed of Sound Using Wavelength
99(1)
6.9.2 Calculate the Speed of Sound Using Frequency
100(1)
6.9.3 Calculate the Experimental Molar-Constant-Volume Heat Capacity
100(1)
6.9.4 Calculate the Theoretical Molar Constant-Volume Heat Capacity
100(1)
6.10 Discussion Questions
101(1)
6.11 Conclusions
101(2)
Chapter the Seventh BC: Bomb Calorimetry
103(16)
7.1 Introduction
103(1)
7.2 Textbook References
104(1)
7.3 Chemicals
104(1)
7.4 Equipment
105(1)
7.5 Safety
106(1)
7.5.1 Bomb Specific Precautions
106(1)
7.6 Procedure
107(6)
7.6.1 Data Acquisition Setup
107(1)
7.6.2 Thermocouple Calibration
108(1)
7.6.3 Testing
108(1)
7.6.4 Calorimeter Calibration
109(1)
7.6.5 Charging the Bomb
110(1)
7.6.6 Firing the Bomb
111(2)
7.6.7 Your Chemical Sample
113(1)
7.7 Waste Disposal
113(1)
7.8 Shut Down
114(1)
7.9 Literature Values
114(1)
7.10 Data Analysis
114(3)
7.10.1 Thermocouple Calibration
114(1)
7.10.2 Calorimeter Calibration
114(2)
7.10.3 Your Chemical Sample
116(1)
7.11 Discussion Questions
117(1)
7.12 Conclusions
117(2)
Chapter the Eighth LV: Liquid-Vapour Phase Diagrams
119(8)
8.1 Introduction
119(1)
8.2 Textbook References
119(1)
8.3 Chemicals
120(1)
8.4 Equipment
120(1)
8.5 Safety
121(1)
8.6 Procedure
121(3)
8.6.1 Setup
121(1)
8.6.2 Refractive Index of a Mixture Calibration Curve
122(1)
8.6.3 Distillation
123(1)
8.7 Waste Disposal
124(1)
8.8 Shut Down
125(1)
8.9 Literature Values
125(1)
8.10 Data Analysis
125(1)
8.10.1 Refractive Index of a Mixture Calibration Curve
125(1)
8.10.2 Phase Diagram
125(1)
8.11 Discussion Questions
126(1)
8.12 Conclusions
126(1)
Chapter the Ninth SL: A Solid-Liquid Phase Diagram
127(10)
9.1 Introduction
127(1)
9.2 Textbook References
128(1)
9.3 Chemicals
128(1)
9.4 Equipment
129(1)
9.5 Safety
129(1)
9.6 Procedure
129(3)
9.6.1 Setup
129(1)
9.6.2 Pure Sample Preparation
130(1)
9.6.3 Melting Point Determination
131(1)
9.6.4 Mixed Samples Preparation
132(1)
9.7 Waste Disposal
132(1)
9.8 Shut Down
133(1)
9.9 Literature Values
133(1)
9.10 Data Analysis
133(1)
9.10.1 Temperature Measurements
133(1)
9.10.2 Phase Diagram
133(1)
9.10.3 Heat of Fusion
134(1)
9.11 Discussion Questions
134(1)
9.12 Conclusions
135(2)
Chapter the Tenth VP: The Vapour Pressure of a Pure Liquid
137(10)
10.1 Introduction
137(1)
10.2 Textbook References
137(1)
10.3 Chemicals
138(1)
10.4 Equipment
138(1)
10.5 Safety
138(1)
10.6 Procedure
139(3)
10.6.1 Setup
139(1)
10.6.2 Creating the Vapour Lock
140(1)
10.6.3 Vapour Pressure Measurement
141(1)
10.7 Waste Disposal
142(1)
10.8 Shut Down
143(1)
10.9 Data Analysis
143(1)
10.10 Discussion Questions
144(1)
10.11 Conclusions
145(2)
Chapter the Eleventh BP: Boiling Point Elevation By a Solid
147(10)
11.1 Introduction
147(1)
11.2 Textbook References
148(1)
11.3 Chemicals
148(1)
11.4 Equipment
148(1)
11.5 Safety
149(1)
11.6 Procedure
149(3)
11.6.1 Setup
150(1)
11.6.2 Boiling Point of the Pure Liquid
150(1)
11.6.3 Boiling Point of the Calibration Solution
151(1)
11.6.4 Boiling Point of the Benzoic Acid Solution
152(1)
11.7 Waste Disposal
152(1)
11.8 Shut Down
152(1)
11.9 Literature Values
153(1)
11.10 Data Analysis
153(2)
11.10.1 Boiling Point of the Calibration Solution
153(1)
11.10.2 Boiling Point of the Benzoic Acid Solution
153(2)
11.11 Discussion Questions
155(1)
11.12 Conclusions
155(2)
Chapter the Twelfth ST: Surface Tension of Solutions
157(10)
12.1 Introduction
157(1)
12.2 Textbook References
157(1)
12.3 Chemicals
157(1)
12.4 Equipment
158(1)
12.5 Safety
158(1)
12.6 Procedure
158(3)
12.6.1 Capillary Cleaning
158(1)
12.6.2 Experiment Setup
159(1)
12.6.3 Capillary Rise Measurement for Pure Water
160(1)
12.6.4 Solution Preparation
160(1)
12.6.5 Capillary Rise Measurement for an Organic Aqueous Solution
161(1)
12.6.6 Capillary Rise Measurement for an Ionic Aqueous Solution
161(1)
12.7 Waste Disposal
161(1)
12.8 Shut Down
162(1)
12.9 Literature Values
162(1)
12.10 Data Analysis
162(2)
12.10.1 Capillary Calibration
163(1)
12.10.2 Capillary Rise Measurements for an Organic Aqueous Solution
163(1)
12.10.3 Capillary Rise Measurements for an Ionic Aqueous Solution
164(1)
12.11 Discussion Questions
164(1)
12.12 Conclusions
165(2)
Chapter the Thirteenth PA: The Physical Adsorption of Gases
167(8)
13.1 Introduction
167(1)
13.2 Textbook References
167(1)
13.3 Chemicals
168(1)
13.4 Equipment
168(1)
13.5 Safety
169(1)
13.6 Procedure
169(2)
13.6.1 Setup
169(1)
13.6.2 Determination of the Apparatus Volume
170(1)
13.6.3 Determination of Gas Adsorption
170(1)
13.7 Waste Disposal
171(1)
13.8 Shut Down
171(1)
13.9 Literature Values
172(1)
13.10 Data Analysis
172(2)
13.11 Discussion Questions
174(1)
13.12 Conclusions
174(1)
Chapter the Fourteenth PG: Viscosity Measurements of Polymers and Gases
175(12)
14.1 Introduction
175(1)
14.2 Textbook References
176(1)
14.3 Chemicals
176(1)
14.4 Equipment
177(1)
14.5 Safety
177(1)
14.6 Procedure
178(4)
14.6.1 Part A---Polymer Viscosities
178(3)
14.6.2 Part B---Gas Viscosities
181(1)
14.7 Waste Disposal
182(1)
14.8 Shut Down
183(1)
14.9 Literature Values
183(1)
14.10 Data Analysis
183(2)
14.10.1 Part A: Polymer Viscosities
184(1)
14.10.2 Part B: Gas Viscosities
185(1)
14.11 Discussion Questions
185(1)
14.12 Conclusions
186(1)
Chapter the Fifteenth TV: The Temperature Dependence of Viscosity of Motor Oils
187(8)
15.1 Introduction
187(1)
15.2 Textbook References
188(1)
15.3 Chemicals
188(1)
15.4 Equipment
188(1)
15.5 Safety
189(1)
15.6 Procedure
189(2)
15.6.1 Setup
189(1)
15.6.2 Calibration
190(1)
15.6.3 Viscosity Measurements
191(1)
15.7 Waste Disposal
191(1)
15.8 Shut Down
192(1)
15.9 Literature Values
192(1)
15.10 Data Analysis
192(2)
15.11 Discussion Questions
194(1)
15.12 Conclusions
194(1)
Chapter the Sixteenth OR: Oscillating Reactions
195(10)
16.1 Introduction
195(1)
16.2 Textbook References
196(1)
16.3 Chemicals
196(1)
16.4 Equipment
197(1)
16.5 Safety
197(1)
16.6 Procedure
198(3)
16.6.1 Setup
198(1)
16.6.2 Reaction Measurements
199(2)
16.7 Waste Disposal
201(1)
16.8 Shut Down
202(1)
16.9 Data Analysis
202(1)
16.10 Discussion Questions
203(1)
16.11 Conclusions
204(1)
Analysis Techniques Problem Set 205(32)
Useful Tables 237