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E-raamat: Compact NMR [De Gruyter e-raamatud]

  • Formaat: 289 pages, 132 Illustrations, color; 11 Illustrations, black and white
  • Sari: De Gruyter Textbook
  • Ilmumisaeg: 29-Jan-2014
  • Kirjastus: De Gruyter
  • ISBN-13: 9783110266719
Teised raamatud teemal:
  • De Gruyter e-raamatud
  • Hind: 1 260,00 €*
  • * hind, mis tagab piiramatu üheaegsete kasutajate arvuga ligipääsu piiramatuks ajaks
  • Formaat: 289 pages, 132 Illustrations, color; 11 Illustrations, black and white
  • Sari: De Gruyter Textbook
  • Ilmumisaeg: 29-Jan-2014
  • Kirjastus: De Gruyter
  • ISBN-13: 9783110266719
Teised raamatud teemal:
The goal of this book is to provide an introduction to the practical use of mobile NMR at a level as basic as the operation of a smart phone. Each description follows the same didactic pattern: introduction, basic theory, pulse sequences and parameters, beginners-level measurements, advanced-level measurements, and data processing. Nuclear Magnetic Resonance (NMR) spectroscopy is the most popular method for chemists to analyze molecular structures while Magnetic Resonance Imaging (MRI) is a non-invasive diagnostic tool for medical doctors that provides high-contrast images of biological tissue depicting the brain function and the beating heart. In both applications large super-conducting magnets are employed which magnetize atomic nuclei of an object positioned inside the magnet. Their circulating motion is interrogated by radio-frequency waves. Depending on the operating mode, the frequency spectrum provides the chemist with molecular information, the medical doctor with anatomic images, while the materials scientist is interested in NMR relaxation parameters, which scale with material properties and determine the contrast in magnetic resonance images. Recent advances in magnet technology led to a variety of small permanent magnets, by which NMR spectra, images, and relaxation parameters can be measured with mobile and low-cost instruments.
Foreword v
List of Symbols ix
List of Acronyms xiii
1 Introduction to NMR 1(17)
1.1 NMR: Nuclear Magnetic Resonance
1(4)
1.2 Mobile NMR
5(3)
1.3 Measuring methods
8(7)
1.4 Hardware
15(1)
1.5 Summary
16(1)
1.6 Further reading
17(1)
2 Hardware setup and operation 18(15)
2.1 Connecting the spectrometer
18(1)
2.2 Test samples
19(1)
2.3 Starting the operating software
19(2)
2.4 Noise level
21(1)
2.5 Tuning and matching
21(2)
2.6 Calibration of the excitation pulse flip angle
23(2)
2.7 Pulse sequences and parameters
25(6)
2.8 Data processing
31(1)
2.9 Summary
32(1)
2.10 Further reading
32(1)
3 Types of measurements 33(62)
3.1 Spin density
33(11)
3.2 Relaxation and diffusion
44(22)
3.3 Imaging
66(12)
3.4 Spectroscopy
78(17)
4 Solutions, emulsions, and suspensions 95(28)
4.1 Solutions
96(10)
4.2 Emulsions
106(8)
4.3 Suspensions
114(9)
5 Polymers and elastomers 123(34)
5.1 Elastomers
125(14)
5.2 Amorphous polymers
139(4)
5.3 Semi crystalline polymers
143(14)
6 Biological tissues 157(28)
6.1 Depth profiling of skin
158(9)
6.2 Anisotropy of tendon by relaxometry
167(7)
6.3 NMR of plants and fruits
174(11)
7 Porous media 185(40)
7.1 Rock and sediments
186(13)
7.2 Soil
199(13)
7.3 Cement and concrete
212(13)
8 Cultural heritage 225(37)
8.1 Painted walls and stone
225(10)
8.2 Easel paintings
235(8)
8.3 Wood
243(7)
8.4 Paper and parchment
250(5)
8.5 Mummies and bones
255(7)
9 Concluding remarks 262(5)
Index 267
Bernhard Blümich, Sabina Haber-Pohlmeier and Wasif Zia, RWTH University, Aachen, Germany.