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E-raamat: Scanning Probe Microscopy [World Scientific e-raamat]

Edited by (A*star, Singapore), Edited by (A*star, Singapore)
  • Formaat: 278 pages
  • Ilmumisaeg: 14-Dec-2010
  • Kirjastus: World Scientific Publishing Co Pte Ltd
  • ISBN-13: 9789814324779
Teised raamatud teemal:
  • World Scientific e-raamat
  • Hind: 124,74 €*
  • * hind, mis tagab piiramatu üheaegsete kasutajate arvuga ligipääsu piiramatuks ajaks
Scanning Probe MicroscopySuurem pilt
  • Formaat: 278 pages
  • Ilmumisaeg: 14-Dec-2010
  • Kirjastus: World Scientific Publishing Co Pte Ltd
  • ISBN-13: 9789814324779
Teised raamatud teemal:
World Scientific e-raamatudRohkem infot World Scientific e-raamatute kohta
Raamatu kodulehekülg: http://www.worldscientific.com/worldscibooks/10.1142/7943#t=toc
Scanning Probe Microscopy (SPM) is the enabling tool for nano(bio)technology, which has opened new vistas in many interdisciplinary research areas. Concomitant with the developments in SPM instrumentation and techniques are new and previously unthought-of opportunities in materials nanofabrication and characterisation. In particular, the developments in addressing and manipulating matter at the level of single atoms or molecules, and studies of biological materials (e.g. live cells, or cell membranes) result in new and exciting discoveries.The rising importance of SPM demands a concise treatment in the form of a book which is accessible to interdisciplinary practitioners. This book highlights recent advances in the field of SPM with sufficient depth and breadth to provide an intellectually stimulating overview of the current state of the art. The book is based on a set of carefully selected original works from renowned contributors on topics that range from atom technology, scanning tunneling spectroscopy of self-assembled nanostructures, SPM probe fabrication, scanning force microscopy applications in biology and materials science down to the single molecule level, novel scanning probe techniques, and nanolithography.The variety of topics underlines the strong interdisciplinary character of SPM related research and the combined expertise of the contributors gives us a unique opportunity to discuss possible future trends in SPM related research. This makes the book not merely a collection of already published material but an enlightening insight into cutting edge research and global SPM research trends.
Preface xiii
1 Nanotip Technology for Scanning Probe Microscopy 1(36)
Moh'd Rezeq
Christian Joachim
1.1 Introduction
1(3)
1.2 Field Electron Microscope (FEM) and Tip Characterization
4(3)
1.3 Field Ion Microscopy (FIM)
7(3)
1.4 Preparation and Characterization of an Atomically Clean Tip in an FIM
10(3)
1.5 Brief Review of Previous Nanotip Fabrication Methods
13(2)
1.5.1 Field–surface melting method and build-up method
13(1)
1.5.2 Deposition of an external metal atom on tips sharpened by ion sputtering
14(1)
1.5.3 Pd-coated tungsten single atom apex
14(1)
1.5.4 Field-enhanced diffusion growth technique
15(1)
1.6 Mechanisms of Nitrogen Adsorption on Metal Surfaces
15(4)
1.7 Controlled Field-Assisted Etching Method for Tip Sharpening
19(9)
1.7.1 Experimental setup and results
19(4)
1.7.2 Tip apex modeling and nanotip reconstruction
23(3)
1.7.3 Controllability and reproducibility of the technique
26(2)
1.8 Field Emission Characteristics of Single Atom Tips
28(1)
1.9 Applications of Nanotips in Scanning Probe Microscopy and Future Trends
29(1)
1.10 Conclusion
30(7)
2 In Situ STM Studies of Molecular Self-Assembly on Surfaces 37(20)
Wei Chen
Andrew T.S. Wee
2.1 Introduction
37(3)
2.1.1 Self-assembly on surface nanotemplates or nanostructured surfaces
38(1)
2.1.2 Self-assembled 2D molecular nanostructures via directional noncovalent or covalent intermolecular interactions
39(1)
2.2 In Situ Ultrahigh Vacuum Scanning Tunneling Microscopy
40(1)
2.3 Self-Assembled C60 Nanostructures on Molecular Surface Nanotemplates
40(6)
2.4 Hydrogen-Bonded 2D Binary Molecular Networks
46(3)
2.5 Conclusion and Perspectives
49(8)
3 Ballistic Electron Emission Microscopy on Hybrid Metal/Organic/Semiconductor Interfaces 57(18)
Cedric Troadec
Kuan Eng Johnson Goh
3.1 Introduction
57(2)
3.2 General Introduction to Ballistic Electron Emission Microscopy
59(3)
3.3 BEEM in Hybrid Metal/Organic/Semiconductor Devices
62(2)
3.3.1 Chemi sorbed molecule
62(2)
3.3.2 Physisorbed molecule
64(1)
3.4 BEEM on Hybrid Au/Pentacene/n-Si Interfaces
64(5)
3.4.1 Density plots of barrier height and transmission
66(3)
3.5 Conclusions and Outlook
69(6)
4 Force—Extension Behavior of Single Polymer Chains by AFM 75(32)
Marina I. Giannotti
Edit Kutnycinszky
G. Julius Vancso
4.1 Introduction
76(1)
4.2 AFM-Based Single Molecule Force Spectroscopy (SMFS)
77(3)
4.3 Elasticity of Individual Macromolecules
80(5)
4.3.1 Fitting the theoretical models to the experimental data
83(2)
4.4 Single Chain AFM Force Spectroscopy of Stimulus-Responsive Polymers
85(13)
4.4.1 Single chain behavior of stimulus-responsive polymers
85(9)
4.4.2 Single molecule optomechanical cycle
94(2)
4.4.3 Realization of a redox-driven single macromolecule motor
96(2)
4.5 Conclusions and Outlook
98(9)
5 Probing Human Disease States Using Atomic Force Microscopy 107(22)
Ang Li
Chwee Teck Lim
5.1 AFM as an Imaging Tool for Biological Applications
108(9)
5.1.1 Basic and advanced imaging modes
108(2)
5.1.2 Current state of technical developments for biological applications
110(3)
5.1.3 AFM imaging study of malaria and Babesia-infected red blood cells
113(2)
5.1.3.1 Malaria pathology: surface morphology as an indicator of the disease state and association with pathology
113(1)
5.1.3.2 Methods and results
113(1)
5.1.3.3 Discussion
114(1)
5.1.4 AFM imaging study of other diseases
115(2)
5.2 AFM as a Force-Sensing Tool (Nano- and Micromechanical Property Measurements Using AFM)
117(6)
5.2.1 Force measurement and property-mapping techniques
117(2)
5.2.2 Nanoindentation of cancer cells as an example
119(3)
5.2.2.1 Background
119(1)
5.2.2.2 Method and results
119(3)
5.2.2.3 Discussion
122(1)
5.2.3 General applications in disease studies using AFM-based force spectroscopy and nanoindentation techniques
122(1)
5.3 Outlook and Insights
123(6)
6 Conducting Atomic Force Microscopy in Liquids 129(24)
Nitya Nand Gosvami
Sean J. O'Shea
6.1 Introduction
130(3)
6.2 Introduction to Conducting Atomic Force Microscopy (C-AFM)
133(1)
6.3 Analysis of C-AFM Data
134(3)
6.4 Boundary Lubrication Studies Using C-AFM
137(6)
6.5 Squeeze-out of Confined Branched Molecules
143(4)
6.6 Conclusions and Outlook
147(6)
7 Dynamic Force Microscopy in Liquid Media 153(34)
Wulf Hofbauer
7.1 Introduction
154(1)
7.2 Instrumentation for Operation in Liquid
155(16)
7.2.1 Cantilever readout
156(6)
7.2.1.1 Effects of laser coherence
157(2)
7.2.1.2 Effect of the laser numerical aperture
159(1)
7.2.1.3 Characterization of noise levels
160(2)
7.2.2 Cantilever excitation
162(5)
7.2.3 Resonance tracking
167(3)
7.2.3.1 Self-excitation
167(1)
7.2.3.2 Excitation by a phase-locked loop
168(2)
7.2.4 Frequency modulation vs. phase modulation
170(1)
7.3 Application Examples
171(12)
7.3.1 Molecular resolution imaging of self-assembled monolayers
171(2)
7.3.2 Spectroscopy and structure of the liquid–solid interface
173(16)
7.3.2.1 Crystalline structure of n-dodecanol on graphite
174(3)
7.3.2.2 Dissipation
177(4)
7.3.2.3 Role of tip shape
181(2)
7.4 Outlook: From Simple Organics to Biology
183(4)
8 Fabrication of Bio- and Nanopatterns by Dip Pen Nanolithography 187(18)
Qiyuan He
Xiaozhu Zhou
Freddy Y.C. Boey
Hua Zhang
8.1 Introduction
187(2)
8.2 Biomolecules
189(4)
8.2.1 DNA
189(1)
8.2.2 Proteins
189(2)
8.2.3 Enzymes
191(1)
8.2.4 In situ growth of peptides
191(1)
8.2.5 Other biomolecules
192(1)
8.3 Variant Possibility of DPN
193(2)
8.3.1 Nanoparticles
193(1)
8.3.2 CNTs
194(1)
8.4 Extension of DPN Capability
195(2)
8.4.1 Electrochemistry
195(1)
8.4.2 "Click" chemistry
195(1)
8.4.3 Photomask
196(1)
8.4.4 Modification of DPN probes
197(1)
8.5 Higher Throughput
197(2)
8.5.1 Parallel DPN
197(1)
8.5.2 Polymer pen lithography
198(1)
8.6 Conclusion
199(6)
9 Atomic Force Microscopy-Based Nano-Oxidation 205(18)
Xian Ning Xie
Hong Jing Chung
Andrew T.S. Wee
9.1 Introduction
205(2)
9.2 Mechanism of Nano-oxidation
207(1)
9.3 Materials Used in Nano-oxidation
208(1)
9.4 Spreading Modes of OH– Oxidants
209(3)
9.5 Aspect Ratio of Nano-oxide
212(2)
9.6 Media Used for Nano-oxidation
214(2)
9.7 Physichemical Properties of Nano-oxide
216(1)
9.8 Applications of Nano-oxidation
217(1)
9.9 Concluding Remarks
218(5)
10 Nanolithography of Organic Films Using Scanning Probe Microscopy 223(32)
Jegadesan Subbiah
Sajini Vadukumpully
Suresh Valiyaveettil
10.1 Introduction
223(24)
10.1.1 Principles of AFM lithography
225(1)
10.1.2 Mechanical probe nanolithography
226(5)
10.1.2.1 Nanofabrication using self-assembled monolayers
227(1)
10.1.2.2 Scanning probe anodization
228(1)
10.1.2.3 Thermomechanical writing
228(1)
10.1.2.4 Dip pen nanolithography
229(2)
10.1.3 Biased probe nanolithography
231(7)
10.1.3.1 Electrostatic nanolithography
231(7)
10.1.4 Electrochemical nanolithography
238(9)
10.1.4.1 Nanopatterning of PVK films
238(3)
10.1.4.2 Nanopatterning of carbazole monomer
241(1)
10.1.4.3 Conductive and thermal properties of patterned films
242(1)
10.1.4.4 Nanopatterning of electroactive copolymer film
243(4)
10.2 Applications and Challenges of AFM Nanolithography
247(8)
Index 255
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