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E-raamat: Thermal Analysis of Polymers, Fundamentals and Applications: Fundamentals and Applications [Wiley Online]

Edited by (School of Process Administration, France), Edited by (Alcon Laboratories, USA)
  • Formaat: 704 pages
  • Ilmumisaeg: 15-May-2009
  • Kirjastus: John Wiley & Sons Inc
  • ISBN-10: 470423838
  • ISBN-13: 9780470423837
  • Wiley Online
  • Hind: 229,38 €*
  • * hind, mis tagab piiramatu üheaegsete kasutajate arvuga ligipääsu piiramatuks ajaks
  • Formaat: 704 pages
  • Ilmumisaeg: 15-May-2009
  • Kirjastus: John Wiley & Sons Inc
  • ISBN-10: 470423838
  • ISBN-13: 9780470423837
  • Presents a solid introduction to thermal analysis, methods, instrumentation, calibration, and application along with the necessary theoretical background.
  • Useful to chemists, physicists, materials scientists, and engineers who are new to thermal analysis techniques, and to existing users of thermal analysis who wish expand their experience to new techniques and applications
  • Topics covered include Differential Scanning Calorimetry and Differential Thermal Analysis (DSC/DTA), Thermogravimetry, Thermomechanical Analysis and Dilatometry, Dynamic Mechanical Analysis, Micro-Thermal Analysis, Hot Stage Microscopy, and Instrumentation.
  • Written by experts in the various areas of thermal analysis
  • Relevant and detailed experiments and examples follow each chapter.
Preface ix
Introduction 1(6)
Joseph D. Menczel
R. Bruce Prime
Patrick K. Gallagher
Differential Scanning Calorimetry (DSC)
7(234)
Joseph D. Menczel
Lawrence Judovits
R. Bruce Prime
Harvey E. Bair
Mike Reading
Steven Swier
Introduction
7(2)
Elements of Thermodynamics in DSC
9(9)
The Basics of Differential Scanning Calorimetry
18(19)
Purity Determination of Low-Molecular-Mass Compounds by DSC
37(4)
Calibration of Differential Scanning Calorimeters
41(11)
Measurement of Heat Capacity
52(6)
Phase Transitions in Amorphous and Crystalline Polymers
58(57)
Fibers
115(8)
Films
123(7)
Thermosets
130(24)
Differential Photocalorimetry (DPC)
154(8)
Fast-Scan DSC
162(6)
Modulated Temperature Differential Scanning Calorimetry (MTDSC)
168(40)
How to Perform DSC Measurements
208(9)
Instrumentation
217(24)
Appendix
225(1)
Abbreviations
225(4)
References
229(12)
Thermogravimetric Analysis (TGA)
241(78)
R. Bruce Prime
Harvey E. Bair
Sergey Vyazovkin
Patrick K. Gallagher
Alan Riga
Introduction
241(1)
Background Principles and Measurement Modes
242(9)
Calibration and Reference Materials
251(5)
Measurements and Analyses
256(21)
Kinetics
277(18)
Selected Applications
295(13)
Instrumentation
308(11)
Appendix
311(1)
Abbreviations
312(2)
References
314(5)
Thermomechanical Analysis (TMA) and Thermodilatometry (TD)
319(68)
Harvey E. Bair
Ali E. Akinay
Joseph D. Menczel
R. Bruce Prime
Michael Jaffe
Introduction
319(1)
Principles and Theory
320(6)
Instrumental
326(6)
Calibration
332(3)
How to Perform a TMA Experiment
335(5)
Key Applications
340(23)
Selected Industrial Applications (with Details of Experimental Conditions)
363(24)
Appendix
378(2)
Abbreviations
380(1)
References
381(6)
Dynamic Mechanical Analysis (DMA)
387(110)
Richard P. Chartoff
Joseph D. Menczel
Steven H. Dillman
Introduction
387(7)
Characterization of Viscoelastic Behavior
394(7)
The Relationship between Time, Temperature, and Frequency
401(9)
Applications of Dynamic Mechanical Analysis
410(14)
Examples of DMA Characterization for Thermoplastics
424(8)
Characteristics of Fibers and Thin Films
432(6)
DMA Characterization Crosslinked Polymers
438(18)
Practical Aspects of Conducting DMA Experiments
456(21)
Commericial DMA Instrumentation
477(20)
Appendix
488(1)
Abbreviations
489(2)
References
491(6)
Dielectric Analysis (DEA)
497(118)
Aglaia Vassilikou-Dova
Ioannis M. Kalogeras
Introduction
497(5)
Theory and Background of Dielectric Analysis
502(18)
Dielectric Techniques
520(8)
Performing Dielectric Experiments
528(10)
Typical Measurements on Poly(Methyl Methacrylate) (PMMA)
538(15)
Dielectric Analysis of Thermoplastics
553(23)
Dielectric Analysis of Thermosets
576(16)
Instrumentation
592(23)
Appendix
599(1)
Abbreviations
599(4)
References
603(12)
Micro- and Nanocale Local Thermal Analysis
615(36)
Valeriy V Gorbunov
David Grandy
Mike Reading
Vladimir V. Tsukruk
Introduction
615(1)
The Atomic Force Microscope
616(2)
Scanning Thermal Microscopy
618(2)
Thermal Probe Design and Spatial Resolution
620(4)
Measuring Thermal Conductivity and Thermal Force-Distance Curves
624(4)
Local Thermal Analysis
628(5)
Performing a Micro/Nanoscale Thermal Analysis Experiment
633(4)
Examples of Micro/Nanoscale Thermal Analysis Applications
637(7)
Overview of Local Thermal Analysis
644(7)
Abbreviations
647(1)
References
648(3)
Index 651
Joseph D. Menczel, PhD, a recognized expert in thermal analysis of polymers with some thirty years of industrial and academic experience, is Assistant Technical Director at Alcon Laboratories. He has researched more than 120 polymeric systems in which he studied calibration of DSCs, glass transition, nucleation, crystallization, melting, stability, mechanical and micro-mechanical properties of polymers, and polymer-water interactions. Dr. Menczel holds six patents and is the author of seventy scholarly papers. He is the author of two chapters in the bookThermal Characterization of Polymeric Materials. In conducting DSC experiments, Dr. Menczel found a crystal/amorphous interface in semicrystalline polymers, which later became known as the rigid amorphous phase. He is also credited with developing the temperature calibration of DSCs for cooling experiments.

R. Bruce Prime, PhD, is a consultant to industry and government and a recognized authority on the cure and properties of cross-linked polymer systems. During his thirty-year career with IBM, he led teams responsible for developing and implementing polymer applications for printer and information storage technologies. He holds four patents and is the author of more than fifty technical papers and the chapter on thermosets in Thermal Characterization of Polymeric Materials. Dr. Prime is a Fellow of SPE and NATAS and was the 1989 recipient of the Mettler-Toledo Award in Thermal Analysis. He maintains the Web site www.primethermosets.com.