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Safety Assessment for Chemical Processes [Kõva köide]

  • Formaat: Hardback, 350 pages, kõrgus x laius: 245x175 mm, kaal: 750 g, Illustrations
  • Ilmumisaeg: 25-Nov-1998
  • Kirjastus: Wiley-VCH Verlag GmbH
  • ISBN-10: 352728852X
  • ISBN-13: 9783527288526
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  • Formaat: Hardback, 350 pages, kõrgus x laius: 245x175 mm, kaal: 750 g, Illustrations
  • Ilmumisaeg: 25-Nov-1998
  • Kirjastus: Wiley-VCH Verlag GmbH
  • ISBN-10: 352728852X
  • ISBN-13: 9783527288526
In spite of the good safety records of chemical plants many people regard chemical production as dangerous because of a few major accidents that have occurred.

A knowledge of at least the fundamentals of chemical safety technology is indispensable for chemists and engineers working in chemical industry. The increasingly stringent legal and administrative requirements can only be answered by more highly qualified employees.

This book combines the author's experience of 15 years of research in the field of chemical safety and 10 years in the chemical industry. It provides newcomers with an easy access to the field and helps practitioners in the chemical industry to answer all questions concerning their daily work with hazardous materials or potentially dangerous chemical plants. The investigation of risks, and preventive measures to be taken to minimize the probability of an accident, as well as its consequences are explained.
Basic Terminology in Loss Prevention
1(10)
General Safety Terms
1(6)
Hazard Potential and Expectable Damage
2(2)
Risk
4(3)
Basic Terminology for Plant/Process Operation
7(4)
Procedure for Process Safety Investigations
11(12)
Scope of Investigation in its Dependence on the Process Development Stage
12(3)
Definition of Significant Plant or Process Modifications
15(1)
Types of Investigations Corresponding to the Life Cycle Progress
16(7)
Test Methods for the Thermal Stability Assessment of Substances and Mixtures
23(48)
Theoretical Considerations for Laboratory Processes
23(5)
Screening-Methods for kg-Scale Processes
28(22)
Difference Thermal Analysis (DTA) and Differential Scanning Calorimetry (DSC)
29(17)
The Carius Tube Test
46(1)
The Miniautoclave Test
47(1)
Open Cup Measuring Techniques
48(2)
Further Basic Assessment Test Methods for kg-Scale Processes
50(9)
The Burning Test for Solids
50(2)
Test on the Ignitability of Solids
52(1)
Flash-point of Liquids
53(4)
Ignition Temperature of Liquids
57(2)
Partial Testing for Explosion Risk
59(7)
Deflagration Testing
66(2)
Assignment of Testing Methods to Process Unit Operations for the kg-Scale
68(2)
References to Other Problems and Test Methods
70(1)
Methods for the Investigation and Assessment of Chemical Reactions
71(168)
Reaction Engineering Fundamentals
71(29)
Stoichiometry and Extent of Reaction
72(2)
Reaction Rate
74(8)
Ideal Reactor Models
82(2)
Introduction of Characteristic Numbers
84(2)
Mass Balances of the Ideal Reactors
86(5)
Sample Solutions for Isothermal Operating Conditions
91(3)
The General Heat Balance of Cooled Ideal Reactors
94(6)
The Heat Explosion Theory
100(9)
Investigation and Assessment of Normal Operating Conditions
109(108)
The Safety Technical Assessment of Normal Operating Conditions
109(1)
Safe Normal Operation of the Cooled CSTR
110(26)
Safe Normal Operation of the Cooled PFTR
136(9)
Safe Normal Operation of Cooled Batch Reactors
145(15)
Safe Normal Operation of the Cooled Semibatch Reactor
160(15)
Special Problems In The Assessment of Normal Operating Conditions
175(1)
Safe Normal Operation of Reactions Under Reflux
176(4)
Safe Normal Operation of Polymerization Reactions
180(12)
Investigation Methods for the Characterization of Normal Operating Conditions
192(2)
Fundamentals of Thermokinetics
194(1)
Reaction Calorimetry
195(11)
Thermokinetic Evaluation of Reaction Calorimetric Measurements
206(11)
Investigation and Assessment of Upset Operating Conditions
217(1)
The Safety Technical Assessment of the Process Design for Upset Operating Conditions
217(13)
Assessment of the CSTR Under Upset Operating Conditions
223(3)
The Assessment of the SBR Under Upset Operating Conditions
226(2)
The Assessment of the BR Under Upset Operating Conditions
228(2)
Methods for the Investigation of Upset Operating Conditions
230(9)
Dust Explosions (Milling, Mixing, Drying)
239(10)
Fundamentals of Dust Explosions
239(2)
Relevant Technical Safety Data
241(4)
Protective Measures Against Dust Explosions
245(4)
Methods for the Identification of Deviations and Their Assessment
249(10)
Qualitative Methods for the Identification of Deviations
250(5)
Checklists [ 85]
250(1)
Preliminary Hazard Analysis [ 86]
251(1)
``What if'' Method
252(1)
HAZOP Analysis [ 87,88]
252(3)
Quantitative Methods for the Identification of Process Deviations
255(3)
Fault-Tree Analysis [ 89]
255(2)
Event Tree Analysis [ 90]
257(1)
Special Methods
258(1)
Plant Technical Safety Concepts
259(34)
Design of Emergency Relief Systems
259(19)
General Fundamentals of Two-Phase Pressure Relief
262(1)
Design According to Leung's Equilibrium Model
263(5)
Design for Multi-Purpose Plants - A Special Problem -
268(1)
The Concept of the Credible Worst Case
269(2)
The Procedure
271(2)
``The Trick''
273(5)
Summary
278(1)
Safe Disposal and Containment of Emergency Relief Streams
278(7)
Assessment of Vent Line Design to and From Relief Devices
279(1)
Catch Tank Design (Knockout Drums)
280(2)
Cyclone Separator with Separate/Integrated Catch Tank
282(3)
Protection Against Explosions by Inertization
285(8)
Description of the Assessment Procedure for Explosion Risk
285(1)
Classification of Protection Measures Against Explosions
286(1)
Fundamentals of Inertization
287(6)
Concluding Remark
293(2)
Literature Index 295(6)
Subject Index 301