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E-raamat: Advanced Nanotechnologies for Detection and Defence against CBRN Agents

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This volume gives a broad overview of advanced technologies for detection and defence against chemical, biological, radiological and nuclear (CBRN) agents. It provides chapters addressing the preparation and characterization of different nanoscale materials (metals, oxides, glasses, polymers, carbon-based, etc.) and their applications in fields related to security and safety. In addition, it presents an interdisciplinary approach as the contributors come from different areas of research, such as physics, chemistry, engineering, materials science and biology. A major feature of the book is the combination of longer chapters introducing the basic knowledge on a certain topic, and shorter contributions highlighting specific applications in different security areas.
Part I: General Topics
1 Roadmapping the Future in Defense and Security: Innovations in Technology Using Multidisciplinary Convergence
3(14)
Ashok Vaseashta
Part II: Material Preparation and Processing
2 Crystalline Thin Layers of BaTiO3 for Gas Sensors Prepared by PLD
17(14)
Tomas Kocourek
Miroslav Jelinek
Vaclav Studnicka
Jan Drahokoupil
3 A Comparative Study of the Morphology of Y-Type Hexaferrite Powders Obtained by Sol-Gel Auto-Combustion and Ultrasonic Co-precipitation
31(6)
Borislava Georgieva
Svetoslav Kolev
Chavdar Ghelev
Tatyana Koutzarova
Daniela Kovacheva
Benedicte Vertruyen
Raphael Closset
4 2D Hybrid Si-, Ti-Nanocomposites for Optoelectronic Devices Manufactured by the Sol-Gel Method
37(6)
G.M. Telbiz
E. Leonenko
G. Gulbinas
P. Manoryk
5 Surface Plasmon Resonance Band of Ion-Synthesized Ag Nanoparticles in High Dose Ag:PMMA Nanocomposite Films
43(6)
T.S. Kavetskyy
M.M. Kravtsiv
G.M. Telbiz
V.I. Nuzhdin
V.F. Valeev
A.L. Stepanov
6 Formation of a Periodic Structure in a Chalcogenide Film Substrate by Silver Ion Implantation
49(6)
T.S. Kavetskyy
K.V. Zubrytska
A.V. Stronski
L.I. Pan'kiv
P. Petkov
V.I. Nuzhdin
V.F. Valeev
A.M. Rogov
Y.N. Osin
A.S. Morozova
A.L. Stepanov
7 Optical Band Gap and Carbon Clusters in PMMA Nanocomposite Films Formed by Ion Implantation: Boron, Helium, and Xenon Ions
55(8)
M. Trzcinski
T.S. Kavetskyy
A.L. Stepanov
Part III: Structural and Optical Characterization
8 Preparation and Characterization of SERS Substrates of Different Morphology
63(6)
I. Rigo
M. Veres
L. Himics
T. Vaczi
P. Furjes
9 Synthesis of UV Sensitive Rare Earth Doped Materials
69(10)
Irena Kostova
Dan Tonchev
10 Characterization of Nickel-Cobaltite Spinel Prepared by Different Methods
79(8)
D. Nicheva
V. Boev
P. Petkov
G. Avdeev
T. Petkova
11 Structure and Thermal Behaviour of Lithium Sodium Sulphate
87(8)
Z. Slavkova
O. Kostadinova
G. Avdeev
T. Petkova
12 Influence of Modification on the Structure and Physical Properties of Arsenic Trisulfide. A Short Review
95(10)
Oleksandr Paiuk
Part IV: Electrical Characterization
13 Time Domain Versus Frequency Domain in the Characterization of Materials
105(16)
L.C. Costa
14 The Measurement of Thermally Stimulated Depolarization and Polarization Currents
121(18)
M.P.F. Graca
P.R. Prezas
15 Iron Concentration Effect on the Microwave Dielectric Properties of BiNbO4 Ceramics
139(14)
S. Devesa
M.P. Graca
L.C. Costa
16 Dielectric Analysis of Phosphate-Borate Glass-Ceramics Doped with Alkali Oxides
153(12)
B.M.G. Melo
M.A. Valente
M.P.F. Graca
17 Electrical and Magnetic Properties of Yttrium Ferrites
165(12)
S. Soreto Teixeira
A.J.M. Sales
M.P.F. Graca
M.A. Valente
L.C. Costa
Part V: Materials: Graphene, Nanotubes and Nanodiamonds
18 Nanostructured Carbon Materials: Synthesis and Applications
177(16)
Alejandro Anson-Casaos
Enrique Garcia-Bordeje
Ana M. Benito
Wolfgang K. Maser
19 Quantum Information Technology and Sensing Based on Color Centers in Diamond
193(22)
Nina Felgen
Alexander Schmidt
Boris Naydenov
Fedor Jelezko
Johann Peter Reithmaier
Cyril Popov
20 Experimental Study of Spectral Parameters of Silicon-Vacancy Centers in MWCVD Nanodiamond Films Important for Sensing Applications
215(6)
L. Himics
M. Veres
S. Toth
I. Rigo
M. Koos
21 Electrochemical Synthesis of PANI/Graphene Nanocomposites Aimed for Sensors
221(8)
Aleksandar Petrovski
Perica Paunovic
Anita Grozdanov
Aleksandar T. Dimitrov
Gennaro Gentile
Maurizio Avella
22 Preparation of Metallic and Semiconducting SWCNT Inks by a Simple Chromatographic Method: A Two-Parameter Study
229(12)
Ana Santidrian
Nekane Lozano
Ana M. Benito
Wolfgang K. Maser
Alejandro Anson-Casaos
Part VI: Materials: Nanowires and Fibers
23 Loaded Nanofibers: Force Protection, Filtration, Decontamination
241(12)
Ashok Vaseashta
Nimet Karagulle-Bolgen
24 Nanocomposites of Electrospun Polymeric Materials As Protective Textiles Against Chemical and Biological Hazards
253(8)
Nimet Bolgen
Ashok Vaseashta
Part VII: Materials: Nanocomposites
25 Temperature Effect on the Dielectric Response of Carbon Nanotubes Particles Filled Polyester Polymer Composites
261(12)
Z. Samir
S. Boukheir
Y. El Merabet
M.P.F. Graca
M.E. Achour
L.C. Costa
26 Nanosized Ferrite Materials for Absorption of and Protection from MW Radiation
273(12)
Svetoslav Kolev
Tatyana Koutzarova
27 Dielectric Relaxation in Biocomposites Based on Olive Pomace Grains
285(8)
L. Kreit
Z. Samir
I. Bouknaitir
A. Triki
M.E. Achour
L.C. Costa
A. Kallel
A. Oueriagli
M. Mabrouki
28 Green Synthesis of Silver Nanoparticles and Their Application in Thin Polymer Films
293(6)
Zhana Petkova
Irena Kostova
Ginka Antova
29 Synthesis of Iron Oxide Nanoparticles Modified with Silanes and Their Heating Ability in Alternating Magnetic Fields
299(10)
L. Storozhuk
N. Iukhymenko
Part VIII: Materials: Glasses and Polymers
30 Ureasil-Based Polymer Matrices As Sensitive Layers for the Construction of Amperometric Biosensors
309(8)
T.S. Kavetskyy
O. Smutok
M. Gonchar
O. Sausa
Y. Kukhazh
H. Svajdlenkova
T. Petkova
V. Boev
V. Ilcheva
31 Impedance Characterization of Gas Sensitive Chalcogenide Films
317(16)
Dumitru Tsiulyanu
Marina Ciobanu
Olga Mocreac
32 Swelling Behavior of Organic-Inorganic Ureasil-Based Polymers
333(6)
T.S. Kavetskyy
H. Svajdlenkova
Y. Kukhazh
O. Sausa
K. Cechova
I. Mat'ko
N. Hoivanovych
O. Dytso
T. Petkova
V. Boev
V. Ilcheva
33 Synthesis and Characterization of Organically Modified Silicates Obtained by Co-condensation of Two Organic-Inorganic Ureasilicate Monomers
339(10)
V. Ilcheva
V. Boev
D. Tatchev
G. Avdeev
G. Zamfirova
V. Gaydarov
V. Lilova
T. Petkova
34 Sr-Substituted Barium Titanate Glass Ceramics from Oxide Glasses As Potential Material for Sensor Preparation
349(12)
Ruzha Harizanova
Liliya Vladislavova
Christian Bocker
Georgi Avdeev
Christian Russel
35 BaO/SrO/ZnO/SiO2 Glass System: Influence of Different Nucleation Agents: Bulk Versus Surface Crystallisation
361(6)
Liliya Vladislavova
Christian Thieme
Tilman Zscheckel
Christian Patzig
Thomas Hoche
Christian Russel
36 Bismuth-Titanate Bi2Ti2O7 Crystallization in the Bi2O3/TiO2/SiO2/Nd2O3 System
367(8)
Stanislav Slavov
Zheng Jiao
Part IX: Applications: Sensors and Detectors
37 Application of Sm Oxide Doped Oxyfluoride Glasses for the Development of Extrinsic Fibre Optical X-Ray Sensors
375(14)
T. Eftimov
D. Tonchev
I. Kostova
G. Patronov
T. Pashova
38 MWCNT/PANI Screen Printed Electrodes for Gas Sensors
389(8)
Gorazd Chepishevski
Aleksandar Petrovski
Anita Grozdanov
Perica Paunovic
Aleksandar Dimitrov
Gennaro Gentile
Maurizio Avella
39 Synthesis of RGO/SiO2 and Ag/RGO/SiO2 Nanocomposites and Study of Their Sensitivity Towards Humidity
397(10)
A.S.A. Shalaby
Sh. Safwat-Mansour
Ahmed S. Afify
M. Hassan
A. Staneva
40 Preparation of Nanoporous Hybrid Materials with Bridged Tetra Sulfide Functional Groups and Determination of Their Sensing Characteristics Towards Relative Humidity
407(10)
M. Abdallah
N. Velikova
Y. Ivanova
Ahmed S. Afify
M. Ataalla
M. Hassan
41 Humidity Sensing Properties of Tungsten Based Glass Crystalline Materials in the WO3-ZnO-La2O3-Al2O3 System
417(10)
M. Ataalla
Ahmed S. Afify
M. Hassan
A.M. Adam
M. Milanova
Iskra Piroeva
42 Green Synthesis of Silver Nanoparticles Using Lantana Camara Leaf Extract and Their Use as Mercury(II) Ion Sensor
427(8)
Didem Demir
Nimet Bolgen
Ashok Vaseashta
43 Highly Ordered AAO Layers for Various Sensor Applications
435(10)
S. Kozhukharov
Ch. Girginov
O. Kostadinova
44 Individual Bi2O3-Functionalized ZnO Microwire for Hydrogen Gas Detection
445(8)
Vasile Postica
Oleg Lupan
Jorit Grottrup
Rainer Adelung
Part X: Applications: Water Treatment, Environment and Health
45 Improvement of the Catalytic Activity of Pt through Synergetic Interaction with Co
453(14)
Perica Paunovic
Orce Popovski
Prashant Khadke
Ulrike Krewer
Goran Nacevski
Anita Grozdanov
Aleksandar T. Dimitrov
46 Antibacterial Coatings for Biomedical Applications
467(10)
P. Pisarik
M. Jelinek
J. Remsa
J. Miksovsky
47 Identification and Evolution of Biocatalysts of Interest
477(10)
Ioannis V. Pavlidis
48 Self-Organized Magnetic Nanoparticles in Plant Systems: ESR Detection and Perspectives for Biomedical Applications
487(6)
T.S. Kavetskyy
R.I. Khalilov
O.O. Voloshanska
L.M. Kropyvnytska
T.M. Beyba
V.A. Serezhenkov
A.N. Nasibova
A. Akbarzadeh
S.Ya. Voloshanska
49 Nanoparticle Based Decontamination of Bacteria/Pathogens
493(6)
N. Enaki
T. Paslari
E. Starodub
S. Bizgan
C. Ristoscu
I.N. Mihailescu
A. Vaseashta
50 Development of Nanostructured Materials with CBRN Agents Sensing Properties
499(10)
A. Stoilova
A. Georgiev
D. Nazarova
L. Nedelchev
D. Dimov
P. Petkov
Index 509
Plamen Petkov received his degree in Physics from the University of Chemical Technology and Metallurgy, Sofia, Bulgaria in 1981 and his PhD in Physics in 1994. He has worked at postdoc positions in I. Physicalisches Institut, RWTH, Aachen, Germany, University of Odense, Denmark, University of Bonn, Germany. Actually, he is a full professor of applied physics at the University of Chemical Technology and Metallurgy and head of Physics Department and Thin Film Technology Laboratory. His research activity is mainly devoted to electrical and optical properties of semiconductor materials for various technological applications. He is author of more than 150 archival refereed journal papers, co-author and co-editor of 5 books, 10 patents and inventions on topics of solid state physics.

Dumitru Tsiulyanu received his degree in Physics from the Institute of Applied Physics at the Moldavian Academy of Science (PhD in 1975 and DSc in 1988). Since 1989 he has worked at the Technical University of Moldova and since 1999 he is Head of the Physics Department and full professor in physics. Present scientific interests include investigations of basic physical properties of chalcogenides and their application development in instrumentation for environmental monitoring. His publication activity includes 150 archival refereed journal papers, co-authorship of 6 books, 20 patents and inventions on the topics of gas sensors and sensor systems.

Cyril Popov received his MSc in Chemical Engineering in 1990 and PhD in 1994 from the University of Chemical Technology and Metallurgy, Sofia, Bulgaria. In the period 1995-1997 he was a Postdoctoral Fellow at the National Institute of Advanced Industrial Science and Technology (AIST), Tsukuba, Japan and at the Central Laboratory of Photoprocesses, Bulgarian Academy of Sciences, Sofia, working on preparation and investigation of novel materials in the ternary system B-C-N. In 1998 he joined the Institute of Nanostructure Technologies and Analytics (INA), University of Kassel, Germany, where at the present he is a Group leader. His current research interests cover deposition, characterization and applications of nano- and ultrananocrystalline diamond films. He is co-author of more than 100 publications, 20 contributions to conference proceedings and 18 book chapters, co-editor of 4 books.

Wilhelm Kulisch studied Physics at the Universities of Münster and Kassel in Germany. Degrees: diploma, PhD and habilition. Since 1988 he works as Researcher and Teacher at the Institute of Nanotechnology (formely Microtechnology) and Analytics at the University of Kassel. His fields of research (among other) include semiconductor devices, thin film technology, superhard materials, diamond and nanodiamond, nanotechnology, biosensors. Between 2003 and 2009 he stayed four years at the NanoBioTech group at the Joint Research Center of the European Commission in Ispra, Italy. He is author of over 200 publications, ca. 10 textbooks and two monographies, editor of five books on diamond and sensors.