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E-raamat: Basic Gas Chromatography

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(Virginia Polytechnic Institute and State University), , (Drew University)
  • Formaat: PDF+DRM
  • Ilmumisaeg: 31-Jul-2019
  • Kirjastus: John Wiley & Sons Inc
  • Keel: eng
  • ISBN-13: 9781119450733
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Basic Gas ChromatographySuurem pilt
  • Formaat: PDF+DRM
  • Ilmumisaeg: 31-Jul-2019
  • Kirjastus: John Wiley & Sons Inc
  • Keel: eng
  • ISBN-13: 9781119450733
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Basic Gas Chromatography, Third Edition provides a brief introduction to GC following the objectives for titles in this series. It should appeal to readers with varying levels of education and emphasizes a practical, applied approach to the subject. : This book provides a quick need-to-know introduction to gas chromatography; still the most widely used instrumental analysis technique, and is intended to assist new users in gaining understanding quickly and as a quick reference for experienced users.

The new edition provides updated chapters that reflect changes in technology and methodology, especially sample preparation, detectors and multidimensional chromatography. The book also covers new detectors recently introduced and sample preparation methods that have become much more easily accessible since the previous edition.
Preface To The Third Edition xi
Preface To The Second Edition xiii
Preface To The First Edition xv
Acknowledgments xvii
1 Introduction
1(14)
A Brief History
1(2)
Definitions
3(6)
Overview: Advantages and Disadvantages
9(3)
Instrumentation and Columns
12(2)
References
14(1)
2 Basic Concepts And Terms
15(22)
Definitions, Terms, and Symbols
15(10)
The Rate Theory
25(9)
The Achievement of Separation
34(1)
References
35(2)
3 Instrument Overview
37(14)
Carrier Gas
38(1)
Flow Control and Measurement
39(3)
Sample Inlets and Sampling Devices
42(4)
Capillary Columns
46(1)
Temperature Zones
47(2)
Detectors
49(1)
Data Systems
50(1)
Reference
50(1)
4 Capillary Columns
51(18)
Types of Capillary Columns
51(3)
Capillary Column Tubing
54(1)
Advantages of Capillary Columns
55(2)
Column Selection
57(8)
Column Quality Testing: The Grob Test Mix
65(1)
Special Troubleshooting Considerations for Capillary Columns
66(1)
Guidelines For Selecting Capillary Columns
67(1)
References
68(1)
5 Stationary Phases
69(18)
Selecting a Column
69(12)
Common and Important Stationary Phases
81(2)
Other Common Stationary Phases
83(3)
References
86(1)
6 Temperature Programming
87(12)
Advantages and Disadvantages of TPGC
89(1)
Requirements for TPGC
90(1)
Example Temperature Programmed Chromatograms
91(5)
Special Topics
96(2)
References
98(1)
7 Inlets
99(14)
Inlet Fundamentals
99(2)
Split Inlet
101(3)
Splitless Inlet
104(2)
On-Column Inlet
106(1)
Programmed Temperature Vaporizer (PTV)
107(1)
Related Topics
108(3)
References
111(2)
8 Classical Detectors: Fid, Tcd, And Ecd
113(26)
Classification of Detectors
115(2)
Common Detector Characteristics
117(7)
Flame Ionization Detector (FID)
124(4)
Thermal Conductivity Detector (TCD)
128(3)
Electron Capture Detector (ECD)
131(3)
Other Detectors
134(2)
References
136(3)
9 Qualitative And Quantitative Analysis
139(18)
Qualitative Analysis
139(6)
Quantitative Analysis
145(1)
Statistics of Quantitative Calculations
145(3)
Quantitative Analysis Methods
148(6)
Summary
154(1)
References
154(3)
10 GC-MS And Spectrometry Detectors
157(20)
Gas Chromatography-Mass Spectrometry (GC-MS)
158(13)
Gas Chromatography-Mass Spectrometry-Mass Spectrometry (GC-MS-MS)
171(1)
Gas Chromatography-Fourier Transform Infrared Spectrometry (GC-FITR)
172(1)
Gas Chromatography-Vacuum Ultraviolet (GC-VUV) Spectrometry
172(2)
References
174(3)
11 Sampling Methods
177(20)
Overview
177(2)
Liquid-Liquid Extraction (LLE)
179(3)
Solid-Liquid Extraction: Soxhlet Extraction and Accelerated Solvent Extraction (ASE)
182(1)
Solid-Phase Extraction
183(3)
Liquid-Vapor or Solid-Vapor Extraction: Headspace Extraction
186(2)
Solid-phase microextraction (SPME)
188(4)
QuEChERS (Quick, Easy Cheap, Effective, Rugged, Safe)
192(1)
Additional Techniques and Summary
193(1)
References
194(3)
12 Multidimensional Gas Chromatography
197(14)
Overview
197(1)
Fundamental Principles of Multidimensional Chromatography
198(4)
Heart Cutting
202(1)
Comprehensive Two-Dimensional GC (GCxGC)
203(3)
LC-GC with Heart Cutting
206(1)
Comprehensive LCxGC
206(2)
References
208(3)
13 Packed Column GC
211(14)
Columns
211(2)
Solid Supports and Stationary Phases
213(1)
Liquid Stationary Phases
214(1)
Solid Stationary Phases
215(3)
Gas Analysis
218(3)
Analysis of Other Inorganics
221(1)
Inlets and Liquid Sampling for Packed Columns
221(1)
Special Columns and Applications
222(2)
References
224(1)
14 Special Topics
225(16)
Fast GC
225(3)
Chiral Analysis by GC
228(1)
Analysis of Nonvolatile Compounds
229(4)
Pyrolysis
233(1)
Inverse GC
233(1)
Additional Theory
234(2)
Activity Coefficients
236(2)
References
238(3)
15 Troubleshooting Gc Systems
241(10)
Preventing Problems
241(2)
Troubleshooting Problems
243(8)
Appendix A Acronyms, Symbols And Greek Symbols 251(4)
Appendix B Some Internet Sites For Gas Chromatography 255(2)
Appendix C Other Books On Gas Chromatography 257(2)
Index 259
HAROLD M. MCNAIR, PHD, is Professor Emeritus of Chemistry at Virginia Tech, and is known internationally as a leading researcher and educator in the field of gas chromatography.

JAMES M. MILLER, PHD, is Professor Emeritus of Chemistry at Drew University, where he taught for 36 years.

NICHOLAS H. SNOW, PHD, is Professor of Chemistry and Biochemistry at Seton Hall University. He is widely published in gas chromatography and has been teaching GC to new students for over 30 years.
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