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E-raamat: Chemistry of High-Energy Materials

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  • Formaat: PDF+DRM
  • Sari: De Gruyter Textbook
  • Ilmumisaeg: 13-Nov-2015
  • Kirjastus: De Gruyter
  • Keel: eng
  • ISBN-13: 9783110439335
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Chemistry of High-Energy MaterialsSuurem pilt
  • Formaat: PDF+DRM
  • Sari: De Gruyter Textbook
  • Ilmumisaeg: 13-Nov-2015
  • Kirjastus: De Gruyter
  • Keel: eng
  • ISBN-13: 9783110439335
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Chemistry of High-Energy Materials continues in this new and revised 3rd edition to provide fundamental scientific insights into primary and secondary explosives, propellants, rocket fuel and pyrotechnics. The contents of the previous edition were meticulously updated and recent research developments added to this graduate-level textbook. Applications in military and civil fields are discussed. Especially environmental issues caused by lead-based primary explosives, perchlorates in pyrotechnic formulations and modern signal flare compositions are discussed and current research presented. Further additions include the understanding of the mechanism and continuing development of laser ignition methods, techniques for the characterization of detonators and their output as well as principles and effects of underwater explosions.



New in the 3rd Edition:



Revised and updated content, new study problems and questions.

Extended examination of the application of ionic liquids in the field and hydrodynamics.

Intended for advanced students in chemistry, materials science and engineering, as well as to all those working in defense technology.

"This book makes a nice addition to the shelf of everyone involved with energetic materials. As such it is recommended as a very useful reference for both students and experienced readers." Ernst-Christian Koch on the 2nd Edition in: Propellants Explosive Pyrotechnics 16/2011

Upcoming titles by Thomas M. Klapötke:





Energetic Materials Encyclopedia (January 2018)



Thomas M. Klapötke

CSci CChem FRSC was from 1995 until 1997 Ramsay Professor of Chemistry at the University of Glasgow in Scotland. Since 1997 he has held the Chair of Inorganic Chemistry at LMU Munich.
Preface to this 3rd English edition vii
Preface to this 2nd English edition viii
Preface to the first English edition ix
Preface to the first German edition x
1 Introduction
1(44)
1.1 Historical Overview
1(9)
1.2 New Developments
10(25)
1.2.1 Polymer-Bonded Explosives
10(3)
1.2.2 New High (Secondary) Explosives
13(10)
1.2.3 New Primary Explosives
23(9)
1.2.4 New Oxidizers for Solid Rocket Motors
32(3)
1.3 Definitions
35(4)
1.4 Combustion, Deflagration, Detonation -- A Short Introduction
39(6)
1.4.1 Fire and Combustion
39(3)
1.4.2 Deflagration and Detonation
42(3)
2 Classification of Energetic Materials
45(54)
2.1 Primary Explosives
45(3)
2.2 High (Secondary) Explosives
48(7)
2.3 Propellant Charges
55(3)
2.4 Rocket Propellants
58(12)
2.4.1 Chemical Thermal Propulsion (CTP)
69(1)
2.5 Pyrotechnics
70(29)
2.5.1 Detonators, Initiators, Delay Compositions and Heat-Generating Pyrotechnics
70(4)
2.5.2 Light-Generating Pyrotechnics
74(7)
2.5.3 Decoy Flares
81(6)
2.5.4 Smoke Munitions
87(9)
2.5.5 Near-Infrared (NIR) Compositions
96(3)
3 Detonation, Detonation Velocity and Detonation Pressure
99(8)
4 Thermodynamics
107(30)
4.1 Theoretical Basis
107(6)
4.2 Computational Methods
113(24)
4.2.1 Thermodynamics
113(3)
4.2.2 Detonation Parameters
116(5)
4.2.3 Combustion Parameters
121(5)
4.2.4 Example: Theoretical Evaluation of New Solid Rocket Propellants
126(7)
4.2.5 Example: EXPLO5 Calculation of the Gun Propellant Properties of Single, Double and Triple Base Propellants
133(4)
5 Initiation
137(12)
5.1 Introduction
137(2)
5.2 Ignition and Initiation of Energetic Materials
139(2)
5.3 Laser Ignition and Initiation
141(8)
6 Experimental Characterization of Explosives
149(16)
6.1 Sensitivities
149(5)
6.2 Long-Term Stabilities
154(2)
6.3 Insensitive Munitions
156(2)
6.4 Gap Test
158(1)
6.5 Classification
159(2)
6.6 Trauzl Test
161(4)
7 Special Aspects of Explosives
165(30)
7.1 Shaped Charges
165(6)
7.2 Detonation Velocities
171(6)
7.3 Gurney Model
177(5)
7.3.1 Example: Calculation of the Gurney Velocity for a General Purpose Bomb
181(1)
7.4 Plate Dent Tests vs. Fragment Velocities
182(7)
7.5 Underwater explosions
189(6)
8 Correlation between the Electrostatic Potential and the Impact Sensitivity
195(6)
8.1 Electrostatic Potentials
195(3)
8.2 Volume-Based Sensitivities
198(3)
9 Design of Novel Energetic Materials
201(36)
9.1 Classification
201(2)
9.2 Polynitrogen Compounds
203(5)
9.3 High-Nitrogen Compounds
208(17)
9.3.1 Tetrazole and Dinitramide Chemistry
209(7)
9.3.2 Tetrazole, Tetrazine and Trinitroethyl Chemistry
216(5)
9.3.3 Ionic Liquids
221(4)
9.4 Dinitroguanidine Derivatives
225(2)
9.5 Co-Crystallization
227(1)
9.6 Future Energetics
228(9)
10 Synthesis of Energetic Materials
237(8)
10.1 Molecular Building Blocks
237(1)
10.2 Nitration Reactions
238(5)
10.3 Processing
243(2)
11 Safe Handling of Energetic Materialsin the Laboratory
245(6)
11.1 General
245(1)
11.2 Protective Equipment
246(3)
11.3 Laboratory Equipment
249(2)
12 Energetic Materials of the Future
251(8)
13 Related Topics
259(14)
13.1 Thermobaric Weapons
259(2)
13.2 Agent Defeat Weapons
261(2)
13.3 Nanothermites
263(9)
13.3.1 Example: Iron Oxide / Aluminum Thermite
269(2)
13.3.2 Example: Copper Oxide / Aluminum Thermite
271(1)
13.3.3 Example: Molybdenum Trioxide / Aluminum Thermite
272(1)
13.4 Homemade Explosives
272(1)
14 Study Questions
273(4)
15 Literature
277(10)
16 Appendix
287(1)
Important reaction types in organic nitrogen chemistry 287(4)
Curing of a diol (HTPB) with isocyanate binder 291(1)
Important reaction types in inorganic nitrogen chemistry 291(10)
Collection of formulas 301(6)
Author 307(2)
Index 309
Thomas M. Klapötke, Ludwig Maximilian University, Munich, Germany.
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