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E-raamat: Polymer Colloids: Formation, Characterization and Applications

Edited by (Princeton University, USA), Edited by (Princeton University, USA)
  • Formaat: EPUB+DRM
  • Sari: Soft Matter Series Volume 9
  • Ilmumisaeg: 02-Dec-2019
  • Kirjastus: Royal Society of Chemistry
  • Keel: eng
  • ISBN-13: 9781839161216
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Polymer Colloids: Formation, Characterization and ApplicationsSuurem pilt
  • Formaat: EPUB+DRM
  • Sari: Soft Matter Series Volume 9
  • Ilmumisaeg: 02-Dec-2019
  • Kirjastus: Royal Society of Chemistry
  • Keel: eng
  • ISBN-13: 9781839161216
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Academic and industrial research around polymer-based colloids is huge. Edited by two world-renowned leaders in polymer science and engineering, this is a fundamental text for the field.

Academic and industrial research around polymer-based colloids is huge, driven both by the development of mature technologies, e.g. latexes for coatings, as well as the advancement of new materials and applications, such as building blocks for 2D/3D structures and medicine. Edited by two world-renowned leaders in polymer science and engineering, this is a fundamental text for the field.

Based on a specialised course by the editors, this book provides the reader with an invaluable single source of reference. The first section describes formation, explaining basic properties of emulsions and dispersion polymerization, microfluidic approaches to produce polymer-based colloids and formation via directed self-assembly. The next section details characterisation methodologies from microscopy and small angle scattering, to surface science and simulations. The final chapters close with applications, including Pickering emulsions and molecular engineering for materials development.

A comprehensive guide to polymer colloids, with contributions by leaders in their respective areas, this book is a must-have for researchers and practitioners working across polymers, soft matter and chemical and molecular engineering.

Based on a specialised course by the editors, this book provides the reader with an invaluable single source of reference on polymer colloids. The first section describes formation, explaining basic properties of emulsions and dispersion polymerization, microfluidic approaches to produce polymer-based colloids and formation via directed self-assembly. The next section details characterisation methodologies from microscopy and small angle scattering, to surface science and simulations. Finally, the book finishes with chapters devoted to applications, including pickering emulsions, active matter, and molecular engineering for materials development.

Based on a specialised course by the editors, this book provides the reader with an invaluable single source of reference on polymer colloids. The first section describes formation, explaining basic properties of emulsions and dispersion polymerization, microfluidic approaches to produce polymer-based colloids and formation via directed self-assembly. The next section details characterisation methodologies from microscopy and small angle scattering, to surface science and simulations. Finally, the book finishes with chapters devoted to applications, including pickering emulsions, active matter, and molecular engineering for materials development.
Section I: Emerging Methods in Polymer Colloid Formation
Chapter 1 Development, Characterization, and Application of Novel High Temperature Thermoplastic and Thermosetting Dispersions
3(27)
D.L. Malotky
D.L. Dermody
D. Schmidt
T.J. Young
M. Kalinowski
1.1 Introduction
3(3)
1.2 Droplet Breakup Theory
6(7)
1.2.1 Classical Droplet Breakup Theory
6(1)
1.2.2 Concentrated Emulsion Systems
7(1)
1.2.3 Beyond Steady State - Transient Breakup
8(1)
1.2.4 Surfactant Effects on Rheology and Droplet Breakup
9(1)
1.2.5 Confined Boundaries and Wall Effects
10(1)
1.2.6 Surfactant Optimization
10(1)
1.2.7 Surfactant Selection for Emulsification in Water at Elevated Temperature
11(2)
1.2.8 Conclusions
13(1)
1.3 Applications
13(12)
1.3.1 Considerations for Design of Aqueous Polyolefin Dispersions and their Applications
15(3)
1.3.2 Hybrid Particles for Optical Hiding
18(2)
1.3.3 Polyolefin Dispersions as Adhesion Promoters for Plastic Substrates
20(3)
1.3.4 Dispersion Enabled Heat Activated Pressure Sensitive Adhesive
23(2)
1.4 Conclusions
25(1)
Acknowledgements
25(1)
References
25(5)
Chapter 2 Synthesis of Core-Shell Polymer-based Colloids
30(31)
Mengchen Wu
Rui Liu
2.1 Introduction
30(2)
2.2 Grafting Approach
32(9)
2.2.1 "Grafting To"
32(2)
2.2.2 "Grafting From"
34(7)
2.3 Polymer Deposition
41(6)
2.3.1 Resin or Polydopamine Coating
41(2)
2.3.2 Biopolymer Coating
43(2)
2.3.3 Layer-by-layer Deposition
45(2)
2.4 Self-assembly
47(6)
2.4.1 Co-precipitation
47(3)
2.4.2 Flash NanoPrecipitation (FNP)
50(1)
2.4.3 Microfluidics
51(2)
2.5 Electro-spraying/Jetting
53(2)
2.5.1 Electro-spraying
53(1)
2.5.2 Electro-jetting
53(1)
2.6 Conclusion
54(1)
Acknowledgements
55(1)
References
55(6)
Chapter 3 Flash Nano-precipitation and -complexation to Produce Polymer Colloids
61(39)
Victoria E. Lee
Douglas M. Scott
Robert K. Prud'homme
Rodney D. Priestley
3.1 Introduction
61(1)
3.2 The Flash NanoPrecipitation Process
62(8)
3.2.1 Polymer Collapse, Nucleation, and Aggregation
62(4)
3.2.2 Solvent and Polymer Choice
66(1)
3.2.3 Mechanism of Stabilization
67(2)
3.2.4 Equipment
69(1)
3.3 Homopolymer Colloids
70(2)
3.3.1 Concentration Effects
70(1)
3.3.2 Mixing Time Effects
71(1)
3.4 Colloids from Homopolymer Blends
72(7)
3.4.1 Janus Particles
75(1)
3.4.2 Patchy Particles
75(3)
3.4.3 Core-Shell Particles
78(1)
3.5 Hybrid Polymer-Inorganic Colloids
79(2)
3.6 Block Copolymer Microphase Separation in Colloids
81(4)
3.6.1 Molecular Weight Effect
81(1)
3.6.2 Blends of Block Copolymers and Homopolymers
82(3)
3.7 Polyelectrolyte Complexation
85(6)
3.7.1 Mechanism of Polyelectrolyte Complexation
85(1)
3.7.2 Effect of Mixing Timescales on PEC Formation
86(2)
3.7.3 Flash NanoComplexation (FNC)
88(1)
3.7.4 Encapsulation via FNC
89(2)
3.8 Summary
91(1)
References
91(9)
Chapter 4 Design and Fabrication of Polymer Microparticles and Capsules Using Microfluidics
100(48)
William N. Sharratt
Joao T. Cabral
4.1 Introduction
100(2)
4.2 Single- and Multi-phase Microfluidics and Devices
102(2)
4.3 Chemical Approaches to Particle Solidification
104(18)
4.3.1 Polymerisation of Monomer-containing Droplets
104(5)
4.3.2 Flow Lithography in Single- (and Multi-)phase Flows
109(5)
4.3.3 Covalent Crosslinking of Polymer-containing Droplets
114(3)
4.3.4 Ionic Crosslinking of (Bio)polymer- containing Droplets
117(2)
4.3.5 Interfacial Complexation for Capsule Formation
119(3)
4.4 Physical Approaches to Particle Solidification
122(16)
4.4.1 Particle Assembly at Interfaces
122(6)
4.4.2 Block Co-polymer Self-assembly in Double Emulsions
128(3)
4.4.3 Solvent Extraction of Polymer-containing Droplets
131(7)
4.5 Summary and Outlook
138(2)
4.5.1 Particle Formation Strategies
139(1)
4.5.2 Scalability
139(1)
4.5.3 Full Process Integration, Feedback and Learning
140(1)
References
140(8)
Chapter 5 Recent Advances in Colloidal Polyelectrolyte Brushes
148(45)
Qingsong Yang
Xiaofeng Niu
Zhinan Fu
Li Li
Xuhong Guo
5.1 Introduction
148(3)
5.2 Generation of Metallic Nanoparticles in SPBs
151(10)
5.2.1 Synthesis of Monometallic Nanoparticles
153(1)
5.2.2 Synthesis of Bimetallic Nanoparticles
154(1)
5.2.3 Catalytic Performance
155(1)
5.2.4 Preparation of Metallic Compound Nanoparticles
156(5)
5.3 Preparation of Organic-Inorganic Hybrid Nanoparticles Tempered by SPBs
161(3)
5.4 Controlled Protein Immobilization in SPBs
164(15)
5.4.1 Interactions Between Protein and SPB
164(4)
5.4.2 Characterization Methods for Protein Immobilization on SPBs
168(5)
5.4.3 Effect of SPB Structure on Protein Immobilization in SPBs
173(2)
5.4.4 Effect of pH and Ionic Strength on Protein Immobilization in SPBs
175(4)
5.5 Conclusion and Perspective
179(4)
References
183(10)
Section II: Recent Advances in Colloid Characterization
Chapter 6 The Advanced Microscopy of Colloids
193(47)
Daniel G. Gregory
Nan Yao
6.1 Introduction
193(1)
6.2 A Brief History of Microscopy
194(2)
6.3 Narrowing our Focus - The Specimen: Colloids
196(1)
6.4 Polymer Colloids
197(1)
6.5 Natural Opals and Colloidal Silica
198(4)
6.5.1 Colloidal Crystals
199(1)
6.5.2 Characterization of Colloids
200(2)
6.6 Basics of Microscopy
202(11)
6.6.1 Microscope Probes
202(1)
6.6.2 The Wave-like Nature of Light, Electrons, and Electromagnetic Radiation
203(2)
6.6.3 Lens Basics
205(1)
6.6.4 Aberrations
206(2)
6.6.5 Apertures
208(1)
6.6.6 Magnification
209(1)
6.6.7 Resolution
209(1)
6.6.8 Diffraction Limit of Resolution
210(1)
6.6.9 Resolution Criteria
211(1)
6.6.10 Inspiration for the Electron, Ion, and X-ray Microscope
212(1)
6.7 The "Spectrum" of Microscopes
213(1)
6.8 Optical Microscopes
213(4)
6.8.1 The Visible Light Microscope
213(2)
6.8.2 The Fluorescence Microscope
215(1)
6.8.3 The Confocal Microscope
216(1)
6.9 The X-ray and Atomic Force Microscopes
217(3)
6.9.1 The X-ray Microscope
217(1)
6.9.2 The Atomic Force Microscope (AFM)
218(2)
6.10 Electron Microscopes
220(10)
6.10.1 Electron Microscopy Background
220(3)
6.10.2 The Scanning Electron Microscope (SEM)
223(1)
6.10.3 The Transmission Electron Microscope (TEM)
224(2)
6.10.4 Scanning Transmission Electron Microscopy (STEM)
226(1)
6.10.5 The Ion Microscope
226(1)
6.10.6 The Focused Ion Beam System
227(2)
6.10.7 The Helium Ion Microscope
229(1)
6.11 Instrument Selection for Colloid Analysis
230(2)
6.12 The Microscopy of Colloids - A Summary
232(1)
References
233(7)
Chapter 7 Simulations in Polymer Colloid Formation
240(23)
Arash Nikoubashman
7.1 Introduction
240(1)
7.2 Particle-based Modeling
241(11)
7.2.1 General Considerations
241(5)
7.2.2 Model Details
246(6)
7.3 Kinetic Monte Carlo Simulations
252(7)
Acknowledgements
259(1)
References
259(4)
Chapter 8 Glass Transition and Crystallization in Colloidal Polymer Nanoparticles
263(26)
Daniele Cangialosi
Aurora Nogales
8.1 Introduction
263(1)
8.2 Glassy Dynamics in Colloidal Polymer Nanoparticles
264(10)
8.2.1 The Glass Transition
265(2)
8.2.2 Glass Transition in Geometrical Confinement
267(1)
8.2.3 Specific Features of the Glass Transition in Colloidal Polymer Nanoparticles
268(3)
8.2.4 Specific Features of Physical Aging in Colloidal Polymer Nanoparticles
271(1)
8.2.5 Connection with Molecular Mobility
272(2)
8.3 Semicrystalline Colloidal Particles
274(7)
8.3.1 Methods for Generation of Nanoparticles from Preformed Semicrystalline Polymers
276(2)
8.3.2 Chain Conformation by Confinement of Polymers in Nanoparticles
278(1)
8.3.3 Modification of Crystallization in Polymer Nanoparticles
279(2)
8.3.4 Polymer Nanocrystals from Crystallizable Nanoparticles
281(1)
8.4 Conclusions
281(1)
Acknowledgements
282(1)
References
283(6)
Chapter 9 Transport of Polymer Colloids in Porous Media
289(36)
Navid Bizmark
Joanna Schneider
Emily de Jong
Sujit S. Datta
9.1 Introduction
289(2)
9.2 Mathematical Modeling
291(5)
9.2.1 Macro-scale Modelling: 1D Continuum Advection-dispersion Equation (ADE)
291(1)
9.2.2 Pore-scale Events: Filtration Theory
292(3)
9.2.3 The Lattice-Boltzmann Method (LBM) and Pore Network Modeling (PNM)
295(1)
9.3 Experiments on Colloidal Particle Transport in Porous Media
296(14)
9.3.1 Macro-scale Studies
296(3)
9.3.2 Indirect Pore-scale Assessments
299(4)
9.3.3 Direct Pore-scale Assessments
303(7)
9.4 Conclusions and Outlook
310(2)
References
312(13)
Section III: Advanced Applications of Polymer Colloids
Chapter 10 Pickering Emulsions Stabilized by Polymer Colloids
325(24)
Yang Lan
Yankai Jia
Daeyeon Lee
10.1 Introduction
325(3)
10.1.1 Emulsions
325(1)
10.1.2 Pickering Emulsions
326(2)
10.2 Pickering Emulsions Stabilized by Anisotropic Homogeneous Particles
328(3)
10.3 Janus-particle Stabilized Pickering Emulsions
331(4)
10.3.1 Janus Particles at Liquid-Liquid Interfaces
332(2)
10.3.2 Thermodynamically Stable Pickering Emulsions Stabilized by Janus Particles
334(1)
10.3.3 Janus Balance
335(1)
10.3.4 Stimuli-responsive Pickering Emulsion Stabilized by Janus Particles
335(1)
10.4 Microgel-stabilized Pickering Emulsions
335(5)
10.4.1 Microgels
335(2)
10.4.2 Stimuli-responsive Pickering Emulsions Stabilized by Microgels
337(1)
10.4.3 Microgels at Liquid-Liquid Interfaces
338(1)
10.4.4 High Internal Phase Emulsions Stabilized by Microgels
339(1)
10.5 Pickering Emulsions Stabilized by Polymer-grafted Particles
340(2)
10.6 Biopolymer Colloid-stabilized Pickering Emulsions
342(2)
10.6.1 Cellulose Nanocrystal-stabilized Pickering Emulsions
342(1)
10.6.2 Protein-stabilized Pickering Emulsions
343(1)
10.6.3 Fat Crystal-stabilized Pickering Emulsions
343(1)
10.7 Conclusions and Outlook
344(1)
References
345(4)
Chapter 11 Latexes for Advanced Coatings
349(9)
J. Klier
S. Trevenen
P.J. Beltramo
11.1 Evolution of Latexes for Advanced Coatings
349(4)
11.1.1 Background
349(1)
11.1.2 Architectural Coatings
350(1)
11.1.3 Industrial Coatings
351(1)
11.1.4 New Technological Applications of Anisotropic Latexes
352(1)
11.2 Experimental
353(1)
11.2.1 Film Formation
353(1)
11.2.2 Sample Preparation
353(1)
11.3 Results and Discussion
354(1)
11.4 Conclusion
355(2)
References
357(1)
Chapter 12 Polymer Colloids Enable Medical Applications
358(41)
Christina Tang
Shani Levit
Michael Zeevi
Chris Vasey
Catherine Fromen
12.1 Introduction
358(2)
12.2 Material Selection
360(5)
12.2.1 Natural Polymers
361(1)
12.2.2 Synthetic Polymers
362(3)
12.3 Responsive Nanoparticle Platforms
365(2)
12.3.1 pH Responsive
365(1)
12.3.2 Temperature Responsive
366(1)
12.3.3 Chemoresponsive Polymer Systems
367(1)
12.4 Processing Methods
367(8)
12.4.1 Bottom-up Methods
367(4)
12.4.2 Top-down Methods
371(4)
12.5 Effect of Physiochemical Properties
375(6)
12.5.1 Size
375(1)
12.5.2 Shape
376(1)
12.5.3 Mechanical Properties
377(1)
12.5.4 Surface Chemistry
377(4)
12.6 Emerging Applications
381(4)
12.6.1 Multifunctional Particles
381(1)
12.6.2 Encapsulation of Biologics
381(1)
12.6.3 Alternative Routes of Administration
382(1)
12.6.4 Immune Engineering
383(2)
12.7 Clinical Translation
385(1)
12.8 Outlook
386(1)
Acknowledgements
386(1)
References
387(12)
Chapter 13 Polymer Colloids for Cosmetics and Personal Care
399(19)
Liangchen Xu
Yao Zhou
Samiul Amin
13.1 Introduction
399(1)
13.2 Key Polymer Colloid Properties
400(4)
13.2.1 Particle Size, Particle Size Distribution
400(1)
13.2.2 Film Formation
401(1)
13.2.3 Adhesion
402(1)
13.2.4 Waterproofing
402(1)
13.2.5 Chemistry Modification
402(1)
13.2.6 Lubrication and Tribology
403(1)
13.3 Applications of Polymer Colloids
404(4)
13.3.1 Facial Makeup
404(1)
13.3.2 Sunscreen
405(1)
13.3.3 Mascara
405(1)
13.3.4 Nail Polish
406(1)
13.3.5 Lipstick, Liquid Lipstick
407(1)
13.3.6 Shampoo and Conditioner
407(1)
13.4 Novel Polymer Particles
408(2)
13.4.1 Janus Particle
408(1)
13.4.2 Amphiphilic Particles
409(1)
13.4.3 Sustainable Particles
409(1)
13.4.4 Smart Particles - Stimuli-responsive Polymers
409(1)
13.5 Environmental and Safety Concerns of Polymer Colloids
410(3)
13.5.1 Health and Safety
410(2)
13.5.2 Environmental Safety
412(1)
13.6 Conclusion
413(1)
References
414(4)
Subject Index 418
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