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E-raamat: Reaction Engineering

(Professor, Chemical Engineering Department, Tianjin University, Tianjin, China), (Staff Research Engineer, Chevron Energy Technol), (Professor of Chemical Engineering, Chemical Engineering Department, Tianjin University, Tianjin, China)
  • Formaat: 676 pages
  • Ilmumisaeg: 14-Jul-2017
  • Kirjastus: Butterworth-Heinemann Inc
  • Keel: eng
  • ISBN-13: 9780124104785
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Reaction EngineeringSuurem pilt
  • Formaat: 676 pages
  • Ilmumisaeg: 14-Jul-2017
  • Kirjastus: Butterworth-Heinemann Inc
  • Keel: eng
  • ISBN-13: 9780124104785
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Reaction Engineering clearly and concisely covers the concepts and models of reaction engineering and then applies them to real-world reactor design. The book emphasizes that the foundation of reaction engineering requires the use of kinetics and transport knowledge to explain and analyze reactor behaviors.

The authors use readily understandable language to cover the subject, leaving readers with a comprehensive guide on how to understand, analyze, and make decisions related to improving chemical reactions and chemical reactor design. Worked examples, and over 20 exercises at the end of each chapter, provide opportunities for readers to practice solving problems related to the content covered in the book.

  • Seamlessly integrates chemical kinetics, reaction engineering, and reactor analysis to provide the foundation for optimizing reactions and reactor design
  • Compares and contrasts three types of ideal reactors, then applies reaction engineering principles to real reactor design
  • Covers advanced topics, like microreactors, reactive distillation, membrane reactors, and fuel cells, providing the reader with a broader appreciation of the applications of reaction engineering principles and methods

Muu info

Make more informed choices in your reactor design by better understanding the concepts and models of reaction engineering and their application
1 Introduction
1(24)
1.1 Chemical Reaction Engineering
1(3)
1.2 Conversion and Yield of Chemical Reactions
4(6)
1.2.1 Extent of Reaction
4(1)
1.2.2 Conversion
5(2)
1.2.3 Yield and Selectivity
7(3)
1.3 Classifications of Chemical Reactors
10(3)
1.4 Operation Modes of Chemical Reactors
13(3)
1.5 Models in Reactor Design
16(3)
1.6 Scale-Up of Industrial Reactors
19(6)
Further Reading
22(1)
Problems
22(3)
2 Fundamentals of Reaction Kinetics
25(70)
2.1 Reaction Rate
26(4)
2.2 Reaction Rate Equations
30(7)
2.3 Effect of Temperature on Reaction Rate
37(7)
2.4 Complex Reactions
44(8)
2.4.1 Conversion Rate and Formation Rate
44(1)
2.4.2 Basic Types of Complex Reactions
45(5)
2.4.3 Reaction Network
50(2)
2.5 Transformation and Integration of Reaction Rate Equations
52(8)
2.5.1 Single Reaction
52(5)
2.5.2 Complex Reactions
57(3)
2.6 Heterogeneous Catalysis and Adsorption
60(7)
2.6.1 Heterogeneous Catalysis
61(1)
2.6.2 Adsorption and Desorption
62(5)
2.7 Kinetics of Heterogeneous Catalytic Reactions
67(10)
2.7.1 Steady-State and Rate-Determining Step Approximation
68(2)
2.7.2 Rate Equations of Heterogeneous Catalytic Reactions
70(7)
2.8 Determination of Kinetic Parameters
77(9)
2.8.1 Integration Method
77(2)
2.8.2 Differential Method
79(7)
2.9 Procedure for Developing Reaction Rate Equation
86(9)
Further Reading
87(1)
Problems
88(7)
3 Tank Reactor
95(66)
3.1 Mass Balance for Tank Reactor
96(1)
3.2 Design Calculation of Isothermal Batch Tank Reactor (Single Reaction)
97(6)
3.2.1 Calculation of Reaction Time and Reactor Volume
98(4)
3.2.2 Optimal Reaction Time
102(1)
3.3 Design Calculation of Isothermal Batch Tank Reactor (Complex Reactions)
103(8)
3.3.1 Parallel Reactions
103(4)
3.3.2 Consecutive Reactions
107(4)
3.4 Reactor Volume for Continuous Tank Reactor (CSTR)
111(4)
3.5 CSTR in Series and Parallel
115(8)
3.5.1 Overview
115(2)
3.5.2 Calculations for Multiple Reactors in Series
117(5)
3.5.3 Optimal Reaction Volume Ratio for CSTR in Series
122(1)
3.6 Yield and Selectivity for Complex Reactions in a Tank Reactor
123(10)
3.6.1 Overall Yield and Overall Selectivity
124(1)
3.6.2 Parallel Reactions
125(4)
3.6.3 Consecutive Reactions
129(4)
3.7 Semibatch Tank Reactor
133(5)
3.8 Nonisothermal Batch Reactor
138(7)
3.9 Steady-State Operation of CSTR
145(16)
3.9.1 Heat Balance for CSTR
145(2)
3.9.2 Steady-States of CSTR
147(4)
Summary
151(1)
Further Reading
152(1)
Problems
153(8)
4 Tubular Reactor
161(52)
4.1 Plug Flow and Mixed Flow Reactor
161(2)
4.2 Design of Isothermal Tubular Reactor
163(15)
4.2.1 Single Reaction
164(4)
4.2.2 Multiple Reactions
168(8)
4.2.3 Pseudo Homogeneous Model
176(2)
4.3 Comparison of Reactor Volumes of Tubular and Tank Reactors
178(6)
4.4 Recycle Reactor
184(1)
4.5 Nonisothermal Tubular Reactor
185(12)
4.5.1 Heat Balance Equation for Tubular Reactor
186(2)
4.5.2 Adiabatic Tubular Reactor
188(5)
4.5.3 Nonadiabatic Nonisothermal Tubular Reactor
193(4)
4.6 Optimal Temperature Progression for Tubular Reactors
197(16)
4.6.1 Single Reaction
198(2)
4.6.2 Complex Reactions
200(3)
Further Reading
203(1)
Problems
203(10)
5 Residence Time Distribution and Flow Models for Reactors
213(52)
5.1 Residence Time Distribution
214(4)
5.1.1 Overview
214(1)
5.1.2 Quantitative Delineation of RTD
215(3)
5.2 Experimental Determination of RTD
218(6)
5.2.1 Pulse Experiments
219(2)
5.2.2 Step Experiments
221(3)
5.3 Statistical Characteristics of RTD
224(4)
5.4 RTD of Ideal Reactors
228(6)
5.4.1 Plug-Flow Model
228(2)
5.4.2 Perfectly-Mixed Flow Model
230(4)
5.5 Nonideal Flow Phenomenon
234(4)
5.6 Nonideal Flow Models
238(13)
5.6.1 Segregation Model
238(4)
5.6.2 Tanks-in-Series Model
242(5)
5.6.3 Axial Dispersion Model
247(4)
5.7 Design of Nonideal Reactors
251(5)
5.8 Mixing of Fluids in Flow Reactors
256(9)
Further Reading
260(1)
Questions and Problems
261(4)
6 Chemical Reaction and Transport Phenomena in Heterogeneous System
265(46)
6.1 Steps in Heterogeneous Reactions
266(4)
6.1.1 Macroscopic Structures and Properties of Solid Catalyst Particles
266(3)
6.1.2 Steps in a Catalytic Reaction
269(1)
6.2 Heat and Mass Transfer Between Bulk Fluid and the Catalyst External Surface
270(9)
6.2.1 Transport Coefficient
270(2)
6.2.2 Concentration and Temperature Difference Between the External Surface of Catalyst and Bulk Fluid
272(3)
6.2.3 Effect of External Diffusion on Heterogeneous Catalytic Reactions
275(4)
6.3 Gas Diffusion in Porous Media
279(2)
6.3.1 Diffusion in Pores
279(1)
6.3.2 Diffusion in Porous Particles
280(1)
6.4 Diffusion and Reaction in Porous Catalysts
281(13)
6.4.1 Reactant Concentration Profile in Porous Catalysts
282(3)
6.4.2 Internal Effectiveness Factor
285(5)
6.4.3 Internal Effectiveness Factor for Non-first Order Reactions
290(2)
6.4.4 Effectiveness Factor Under the Influences of Both Internal and External Diffusions
292(2)
6.5 The Effect of Internal Diffusion on Selectivity of Complex Reactions
294(3)
6.6 Determination of Diffusion Impact on Heterogeneous Reactions
297(4)
6.6.1 Determination of the Effects of External Diffusion
297(2)
6.6.2 Determining the Effects of Internal Diffusion
299(2)
6.7 Effects of Diffusion on Experimental Measurement of Reaction Rate
301(10)
Further Reading
305(1)
Problems
306(5)
7 Analysis and Design of Heterogeneous Catalytic Reactors
311(58)
7.1 Transport Phenomena Inside Fixed Bed Reactors
312(8)
7.1.1 Fluid Flow Inside a Fixed Bed
312(4)
7.1.2 Mass and Heat Dispersion Along Axial Direction
316(1)
7.1.3 Mass and Heat Transfer in Radial Direction
317(3)
7.2 Mathematical Model for Fixed Bed Reactor
320(5)
7.3 Adiabatic Fixed Bed Reactor
325(12)
7.3.1 Adiabatic Reactors
325(2)
7.3.2 Catalyst Volume for Adiabatic Fixed Bed Reactor
327(4)
7.3.3 Multistage Adiabatic Reactors
331(6)
7.4 Fixed Bed Reactor With Internal Heat Exchanger
337(10)
7.4.1 Overview
337(2)
7.4.2 Analysis for Single Reaction
339(3)
7.4.3 Analysis of Complex Reaction Systems
342(5)
7.5 Autothermal Fixed Bed Reactors
347(4)
7.5.1 Feed Flow Direction
348(1)
7.5.2 Mathematical Model
349(2)
7.6 Parameter Sensitivity
351(4)
7.7 Laboratory Catalytic Reactor
355(14)
7.7.1 Basic Requirements
355(2)
7.7.2 Main Types of Experimental Reactor
357(4)
Further Reading
361(1)
Problems
361(8)
8 Fluidized Bed Reactor
369(36)
8.1 Introduction
369(1)
8.2 Fluidization
369(7)
8.2.1 Fluidization Phenomenon
369(1)
8.2.2 Particle Classifications
370(1)
8.2.3 Fluidization Parameters
371(4)
8.2.4 Fluidization Regimes
375(1)
8.3 Bubbling Fluidized Bed
376(12)
8.3.1 Bubble Behaviors
377(3)
8.3.2 Mathematical Model of Bubbling Fluidized Bed
380(8)
8.4 Turbulent Fluidized Bed
388(1)
8.4.1 Regime Transition
388(1)
8.4.2 Hydrodynamic Characteristics
389(1)
8.5 Circulating Fluidized Bed
389(9)
8.5.1 Introduction
389(2)
8.5.2 Configuration of CFB
391(1)
8.5.3 Mathematical Models of CFB
392(6)
8.6 Downer Reactor
398(7)
Further Reading
401(1)
Problems
402(3)
9 Multiple-Phase Reactors
405(40)
9.1 Gas--Liquid Reactions
405(7)
9.1.1 Pseudo First Order Reaction
408(4)
9.2 Gas--Liquid Reactors
412(9)
9.2.1 Main Types of Reactors
412(2)
9.2.2 Design of Bubble Column Reactor
414(5)
9.2.3 Design of Stirred Tank Reactor
419(2)
9.3 Gas--Liquid--Solid Reactions
421(4)
9.3.1 Introduction
421(1)
9.3.2 Mass Transfer Steps and Rates in Gas--Solid--Liquid Catalytic Reactions
422(3)
9.4 Trickle Bed Reactors
425(6)
9.4.1 Introduction
425(2)
9.4.2 Mathematical Model
427(4)
9.5 Slurry Reactor
431(14)
9.5.1 Types of Reactors
431(1)
9.5.2 Mass Transfer and Reaction
432(5)
9.5.3 Design of Mechanically Stirred Slurry Tank Reactor
437(4)
Further Reading
441(1)
Problems
441(4)
10 Fluid--Solid Noncatalytic Reaction Kinetics and Reactors
445(46)
10.1 Fluid-Solid Noncatalytic Reactions and Their Applications
446(2)
10.2 Reaction Rate of Particles in Different Shapes
448(3)
10.3 Theoretical Models of Solid Reactions
451(1)
10.4 Kinetic Analysis of Continuous Model
452(2)
10.5 Kinetic Analysis at Constant Particle Size Using the Shrinking Core Model
454(12)
10.5.1 Overall Macroreaction Rate
456(3)
10.5.2 Macroreaction Rate Under Internal Diffusion Control
459(1)
10.5.3 Macroreaction Rate Under External Diffusion Control
460(1)
10.5.4 Intrinsic Reaction Rate Under Surface Reaction Control
461(2)
10.5.5 Comparison and Differentiation of Rate-Controlling Steps at Constant Particle Size
463(3)
10.6 Kinetic Analysis With Changing Particle Diameter Using the Shrinking Core Model
466(7)
10.6.1 Internal Diffusion Control
469(1)
10.6.2 External Diffusion Control
470(1)
10.6.3 Chemical Reaction Control
471(2)
10.6.4 Overall Reaction Time
473(1)
10.7 Microparticle Model
473(4)
10.8 Chemical Vapor Deposition
477(2)
10.9 Design of Fluid--Solid Noncatalytic Reactor
479(12)
10.9.1 Reactor Types
480(1)
10.9.2 Flowing and Mixing of Reaction Components
480(3)
10.9.3 Reactor Design When Fluid Is a Complete Mixing Flow and Solid Phase Is a Plug Flow
483(1)
10.9.4 Reactor Design When Fluid and Solid Phases Can Be Treated as Complete Mixing Flow
484(3)
Further Reading
487(1)
Problems
487(4)
11 Fundamentals of Biochemical Reaction Engineering
491(50)
11.1 Introduction
491(3)
11.2 Fundamentals of Biochemical Reaction Kinetics
494(19)
11.2.1 Enzyme-Catalyzed Reactions and Its Kinetics
494(13)
11.2.2 Kinetics of Microbial Reactions
507(6)
11.3 Immobilized Biocatalysts
513(8)
11.3.1 Introduction
513(1)
11.3.2 Enzyme and Cell Immobilization
514(3)
11.3.3 Catalytic Kinetics of Immobilized Biocatalyst
517(4)
11.4 Bioreactors
521(20)
11.4.1 Types of Bioreactors
522(5)
11.4.2 Bioreactor Calculations
527(9)
Reference
536(1)
Further Reading
536(1)
Problems
536(5)
12 Fundamentals of Polymerization Reaction Engineering
541(58)
12.1 Overview
542(2)
12.2 Kinetics Analysis
544(41)
12.2.1 Polymerization Reaction Types
544(1)
12.2.2 Degree of Polymerization and Distribution
545(8)
12.2.3 Homogeneous Free Radical Polymerization Reaction
553(23)
12.2.4 Polycondensation Reaction
576(6)
12.2.5 Factors That Influence Polymerization Rate
582(3)
12.3 The Analysis of Heat Transfer and Mass Transfer in the Polymerization Process
585(4)
12.3.1 Thermal Effect in the Polymerization Process
585(2)
12.3.2 Heat Transfer and Fluid Flow in the Polymerization Process
587(2)
12.3.3 Heat and Mass Transfer Coefficients
589(1)
12.4 Design and Analysis of Polymerization Reactor
589(10)
12.4.1 Polymerization Reactor and Agitator
589(1)
12.4.2 Mathematical Model
590(1)
12.4.3 Calculation and Analysis of Polymerization Reactors
591(5)
References
596(1)
Further Reading
596(1)
Problems
597(2)
13 Introduction to Electrochemical Reaction Engineering
599(54)
13.1 Introduction
599(9)
13.1.1 Characters of Electrochemical Reactions
599(2)
13.1.2 Performance Parameters for Electrochemical Reaction Engineering
601(7)
13.2 Special Issues in Electrochemical Reaction Engineering
608(21)
13.2.1 Electrical Potential and Current Distribution on Electrode Surface
608(10)
13.2.2 Effects of Gassing
618(4)
13.2.3 Mass Transfer in Electrochemical Engineering
622(3)
13.2.4 Heat Transfer and Balance in Electrochemical Engineering
625(4)
13.3 Electrochemical Reactors
629(24)
13.3.1 Types of Electrochemical Reactors
630(3)
13.3.2 Operation Characters of Electrochemical Reactors
633(12)
13.3.3 Connections and Combination of Electrochemical Reactors
645(5)
References
650(1)
Further Reading
651(1)
Problems
651(2)
Index 653
Prof. Li was a distinguished teacher in China and twice won the state excellence teaching award. His book, Reaction Engineering”, won the highest award in the excellence undergraduate textbook category, an award organized by the Ministry of Education of Peoples Republic of China in 2002. Li has published three textbooks about chemical reaction kinetics and reaction engineering, and more than 70 research papers in the field of reaction engineering. Prof Xin has taught the reaction engineering course since 1997 at Tianjin University and is in charge of the State Elite Course. His research focuses on reaction engineering, on which he has published more than 60 papers. Lin Li, Staff Research Engineer at Chevron Energy Technology Company, Richmond, CA. PhD in Chemical Engineering from Tianjin University, Tianjin, China, 1989. Worked 9 years at Dept. of Chemical Engineering at Tsinghua University, Beijing, China. He moved to the US in 1998, and after research experiences at Princeton University and UC Berkeley he joined UOP, Des Plaines, IL, in 2001 as R & D Specialist. He has published 1 book, more than 40 journal papers and many technical presentations. He also has 4 Chinese patents, and 12 US patent/applications.
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